Bemerkungen: Der erste Vorlesungstag ist der 19.10.2017; in dieser VL-Stunde werden auch die Termine besprochen.
Typ: | Vorlesung (V) | ||
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Semester: | WS 17/18 | ||
Zeit: | 19.10.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 26.10.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 02.11.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 09.11.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 16.11.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 23.11.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 30.11.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 07.12.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 14.12.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 21.12.2017 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 11.01.2018 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 18.01.2018 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 25.01.2018 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 01.02.2018 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik 08.02.2018 13:15 - 14:45 wöchentlich 11.21 Raum 006 11.21 Chemische Technik |
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Dozent: | Prof. Dr. Jan-Dierk Grunwaldt |
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SWS: | 2 | ||
LVNr.: | 5439 | ||
Bemerkungen: Der erste Vorlesungstag ist der 19.10.2017; in dieser VL-Stunde werden auch die Termine besprochen.
Course description
For a targeted design of materials such as catalysts, functional materials and sensors, a good knowledge of the correlation between structure and function are required. The characterization methods which are available are discussed in this advanced course. The main methods comprise TPR, TPD, chemisorption, thermal gravimetry, IR-, Raman-, TEM, XPS and X-ray diffraction. The methods are presented together with practical examples. Finally, synchrotron methods like X-ray absorption spectroscopy (XAS), X-ray emission (XES) and synchrotron X-ray scattering methods are of strong relevance. In all the functional materials discussed in the course the investigation under reaction conditions is of strong importance to understand their structure in its „working“ state.
Organization: AK Prof. Dr. Jan-Dierk Grunwaldt
Location: Room 006, Building 11.21
Time: Every Thursday during the semester, starting on 19.10.2017 at 13.15 h
Registration: not required
Guest lecturer: will be announced
- Introduction, Lecturer (Download): Jan-Dierk Grunwaldt
- UV-vis spectroscopy (Download), Lecturer: Thomas Sheppard
- BET, Chemisorption, TPR (Download), Lecturer: Maria Casapu
- X-ray photoelectron spectroscopy (XPS) (Download), Lecturer: Jan-Dierk Grunwaldt
- Raman spectroscopy (Download), Lecturer: Paul Sprenger
- Infrared spectroscopy (Download), Lecturer: Dmitry Doronkin
- X-ray diffraction (XRD) (Download), Lecturer: Sabrina Müller, Anna Zimina
- Transmission electron microscopy (Download), Lecturer: Reinhard Schneider
- Thermal analysis, Puls-TA, Lecturer: Maria Casapu
- Introduction to X-ray absorption spectroscopy (XAS) (Download), Lecturer: Anna Zimina
- X-ray absorption spectroscopy: XANES/EXAFS (Download), Lecturer: Henning Lichtnberg
- X-ray microscopy (XRM) (Download), Lecturer: Thomas Sheppard
- Operando spectroscopy, Lecturer: Jan-Dierk Grunwaldt
- Small angle X-ray scattering (SAXS), Lecturer: Henning Lichtenberg
Last update: 18.01.2018
To be announced
- Block course, XAS hands-on (1-2 days)
- Introduction, Lecturer: Henning Lichtenberg (Download); UV-vis spectroscopy, Lecturer: Thomas Sheppard (Download)
- BET, Chemisorption, TPR, Lecturer: Maria Casapu (Download)
- Infrared spectroscopy, Lecturer: Jan-Dierk Grunwaldt (Download)
- Raman spectroscopy, Lecturer: Paul Sprenger (Download)
- Surface analysis (XPS, ISS), Lecturer: Jan-Dierk Grunwaldt (Download)
- X-ray diffraction (XRD) - Theory, In situ spectroscopy, synchrotron radition based, Lecturer: Dmitry Doronkin (Download)
- Thermal analysis, Puls-TA, Lecturer: Maria Casapu (Download)
- Electron microscopy (TEM, STEM, etc.), Guest Lecturer: Di Wang (INT, Download)
- Introduction XAS/ EXAFS, Lecturer: Henning Lichtenberg, Abhijeet Gaur (Download)
- Operando spectroscopy, Lecturer Jan-Dierk Grunwaldt (Download)
- Small angle X-ray scattering (SAXS) and X-ray microscopy (XRM), Lecturer: Henning Lichtenberg, Anna Zimina, Jan-Dierk Grunwaldt, Thomas Sheppard
To be announced
- Block course, XAS hands-on (1-2 days)
Last update: 05.11.2016
21.10.2015
- Introduction (Download), Lecturer: Henning Lichtenberg ; UV-vis spectroscopy (Download), Lecturer: Thomas Sheppard
28.10.2015
- BET, Chemisorption, TPR (Download), Lecturer: Jan-Dierk Grunwaldt
04.11.2015
- Electron microscopy, energy-disp. X-ray spectroscopy, EELS Part 1 (Download), Lecturer: Reinhard Schneider
11.11.2015
- Electron microscopy, energy-disp. X-ray spectroscopy, EELS - Part 2, (Download), Lecturer: Reinhard Schneider
18.11.2015
- Infrared spectroscopy (Download), Lecturer: Andreas Gänzler
25.11.2015
- Raman spectroscopy (Download), Lecturer: Paul Sprenger
02.12.2015
- Thermal analysis, Puls-TA (Download), Lecturer: Maria Casapu
09.12.2015
- XRD (Theory, In situ, SR) (Download), Lecturer: Dmitry Doronkin (Anna Zimina)
16.12.2015
- XPS (Download), Lecturer: Ghazal Tofighi, Jan-Dierk Grunwaldt
13.01.2016
- Introduction XAS/ EXAFS (Download), Lecturer: Henning Lichtenberg, Abhijeet Gaur
20.01.2016
- XANES, XES, RIXS (Download), Lecturer: Federico Benzi, Abhijeet Gaur, Henning Lichtenberg
27.01.2016
- SAXS (Download), EPR, NMR (Download), Lecturer: Henning Lichtenberg, Dmitry Doronkin
03.02.2016
- XRM (Download), Lecturer: Sina Baier
10.02.2016
- Operando (Download), Lecturer: Jan-Dierk Grunwaldt
Last update: 09.02.2016
17.02.2014 Overview, Chemisorption, Surface and Thermal Methods, Electron microscopy
- Short overview (Download, Update 16.02.2014)
- Physisorption (BET), Chemisorption, Temperature programmed methods like TPR
(Download, Update 17.02.2014)
- Electron microscopy, scattering methods, synchrotron radiation sources(download)
- Electron Microscopy and related methods: TEM, SEM, STEM-EDX, in situ electron microscopy
18.02.2014 Synchrotron radiation, X-ray microscopy and powder X-ray diffraction
- Synchrotron radiation and synchrotron sources (download)
- X-ray microscopy (download)
- Powder X-ray diffraction
- In situ XRD and synchrotron radiation XRD (download)
19.02.2014 Vibrational methods, UV-vis spectroscopy and surface aalysis
- Infrared spectroscopy (download)
- Raman spectroscopy (download)
- UV-vis spectroscopy (download)
- Surface analysis and X-ray photoelectron spectroscopy
20.02.2014 X-ray absorption spectroscopy and related methods
Preparation: Athena program of the IFFEFIT software (ifeffit-1.2.11), which can be downloaded at http://cars9.uchicago.edu/ifeffit/Downloads.
- Introduction to XAS and EXAFS
- Near edge spectra and X-ray emission: XANES, XES, RIXS
- Block on EXAFS analysis
21.02.2014 Further spectroscopic methods and in situ spectroscopy
- Mößbauer spectroscopy
- EPR spectroscopy
- Thermal analysis, Puls-TA
- In situ studies, in situ cell design and in operando spectroscopy
Final remarks