Institute for Chemical Technology and Polymer Chemistry

Zusatzinformationen: Charakterisierungsmethoden an Synchrotronstrahlungsquellen - Physikalisch-chemische Grundlagen und Anwendungen in der Katalyse

Plan of the current course (SS 2019)

Der Kursus-Plan (regelmäßige Vorlesungen oder Blockkursus) wird am ersten Tag (23.04.2019) besprochen. Falls Sie nicht kommen können, schreiben Sie bitte eine Email an: Prof. Dr. Jan-Dierk Grunwaldt

The plan of the course will be discussed on the first day (regular lessons or block course). If you cannot come on the first date please write an Email to: Prof. Dr. Jan-Dierk Grunwaldt

Slides of the first hour for download: here

 

BIKE Workshop 4: Catalyst characterization and operando spectroscopy

Organizers: Prof. Dr. Jan-Dierk Grunwaldt (KIT) •  Dr. Anna Zimina (KIT) •  Dr. Maria Casapu (KIT)

BIKE project (https://www.bike-msca.eu/) aims at developing and applying, by an innovative “holistic” approach, the next generation of bimetallic catalysts for energy management, in particular for blue and green hydrogen production processes. In this regard, the knowledge-based development of catalysts is a key to a sustainable progress. Understanding their structural dynamics under reaction and operating conditions is mandatory for the identification of the most active species. Hence, the application of advanced in situ/operando characterization methods represents an essential step.

The workshop will offer a comprehensive overview on the different X-ray spectroscopic methods applied in catalysis, with focus on synchrotron-related methods. By involving experts from complementary disciplines it will cover both fundamental and practical aspects as well as current strategies for elucidating various scientific questions.

 

Contributions

Introduction into the course & Welcome

M. Casapu, J.-D. Grunwaldt and A. Zimina, KIT

Synchrotron radiation & synchrotron light sources , introduction to XAS

J.-D. Grunwaldt, Chemical Technology and Catalysis, KIT

X-ray absorption spectroscopy, X-ray absorption near edge structure, LCA, PCA, MCR-ALS

V. Briois, Soleil, https://www.synchrotron-soleil.fr/en/beamlines/rock

Introduction to XAS data analysis

D. Doronkin, Institute for Catalysis Research and Technology, KIT

Advanced EXAFS analysis using atomistic simulations (MD & RMC)

A. Kuzmin, ISSPUL, http://www.dragon.lv/exafs/index.htm

X-ray photo electron spectroscopy

J. Llorca, UPC, Institute of Energy Technologies. https://inte.upc.edu/en/services/laboratories/nemen

Spatially resolved XAS, X-ray microscopy, X-ray tomography

Th. Sheppard, Institute for Catalysis Research and Technology, KIT

Operando studies, engineering of cell design, time resolved studies, combination of methods (XRD, IR, RAMAN)

J.-D. Grunwaldt, Chemical Technology and Catalysis, KIT

Operando XAS

M. Rønning, Norwegian University of Science and Technology  NTNU,  https://www.ntnu.edu/

CATACT: The Catalysis Actinide Beamline at KIT

A. Zimina, Institute for Catalysis Research and Technology, KIT

Introduction to photon-in/photon-out spectroscopy

P. Glatzel, ESRF, https://www.esrf.eu/

 

Tentative Agenda

14.01.2021

9:00 – 9:15

Introduction into the course & Welcome

M. Casapu

J.-D. Grunwaldt

A. Zimina

9:15 – 10:30

Synchrotron radiation & synchrotron light sources , introduction to XAS

J.-D. Grunwaldt

10:30 - 11:00

Coffee break

11:00 - 12:30

X-ray absorption spectroscopy, X-ray absorption near edge structure, LCA, PCA, MCR-ALS

V. Briois

12:30-13:30

Lunch

13:30-15:00

Introduction to XAS data analysis

D. Doronkin

15:00 - 15:30

Coffee break

15:30-17:00

Advanced EXAFS analysis using atomistic simulations (MD & RMC)

A. Kuzmin

15.01.2021

8:30-9:30

X-ray photo electron spectroscopy

J. Llorca

9:30-10:30

Spatially resolved XAS, X-ray microscopy, X-ray tomography

Th. Sheppard

10:30 - 11:00

Coffee break

11:00-12:00

Operando studies, engineering of cell design, time resolved studies, combination of methods (XRD, IR, RAMAN)

J.-D. Grunwaldt

12:00-13:00

Lunch

13:00 – 14:00

Operando XAS in aqueous phase reforming and other energy related processes

M. Rønning

14:00 - 14:30

Coffee break

14:30-16:00

CATACT: The Catalysis Actinide Beamline at KIT

A. Zimina

Closing remarks

J-.D. Grunwaldt

20.01.2020*

tbd

Introduction to photon-in/photon-out spectroscopy

P. Glatzel

tbd

Discussion on studies in BIKE (BIKE intern)

For further information please mail us!

 

Previous courses

Plan for a previous course (SS 2017) and files for download (password-protected):

Overview on the Course 5442 Spektroskopie und Beugungsmethoden am Synchrotron; Physikalisch-chemische Grundlagen und Anwendungen in der Katalyse (SS 2017, Grunwaldt & Lichtenberg)

Course material is only to be used for personal usage.

 

26.04.2017 Synchrotron radiation & synchrotron light sources (Download)
10.05.2017 Introduction to XAS, EXAFS, CAT-ACT (Download)
24.05.2017 XANES, XES, RIXS (Download)
07.06.2017 Tomography, X-ray Microscopy Surface Analysis by XPS in the Lab & with SR (Download)
21.06.217 Time resolved XAS (QEXAFS/DEXAFS) and in situ cell design, spatially resolved XAS, Modulation excitation
05.07.2017 Raman Spectroscopy combined with XAS, operando-spectroscopy SAXS (Download)
19.07.2017 IR combined with XAS, XRD/ED-XRD (Download 1, Download 2)
26.07.2017 Visit to ANKA / Soft X-ray Spectroscopy
18./19.09. Block Course: XAS data Analysis (Hand on) at CAT-ACT workshop

 



Plan for a previous course (WS 2014/2015) and files for download (password-protected):

Course material is only to be used for personal usage.

22.10.2014 Synchrotron radiation & synchrotron light sources (Download Introduction, Synchrotron radiation)
29.10.2014 New CAT-ACT beamline (Download)
05.11.2014 X-ray absorption & X-ray fluorescence, Introduction to XAS (Download)
12.11.2014 X-ray absorption near edge and X-ray emission spectroscopy (XANES, XES, RIXS, Download)
19.11.2014 Introduction to XAS data analysis (Download)
26.11.2014 XANES/EXAFS data analysis exercises
03.12.2014 In situ (operando)studies and cell design (Download)
10.12.2014 Spatially resolved XAS (Download), X-ray microscopy (Download)
17.12.2014 XRD /In situ XRD ( ...using synchrotron rad., data analysis, applications in catalysis, download)
14.01.2015 IR spectroscopy (combined with XAS, download), SAXS (download)
21.01.2015 Raman spectroscopy (combined with XAS, download)
28.01.2015 Surface analysis by XPS: From the lab to synchrotron radiation based studies (download)
04.02.2015 Soft x-ray absorption and emission spectroscopy: experimental methods, in situ applications (Lothar Weinhardt, Clemens Heske, download)
11.02.2015 Visit to ANKA (Meeting point: Busstop campus south 8.25 h or main gate, campus north, 8:50, please contact the lecturers beforehand to get Access)
   
Plan for a previous course (SS 2016) and files for download (password-protected):
20.04.2016 Welcome; Synchrotron radiation & synchrotron light sources (Download)
26.04.2016 X-ray absorption & X-ray fluorescence, Introduction to XAS (Download)
11.05.2016 X-ray absorption near edge and X-ray emission spectroscopy (XANES, XES, RIXS, etc.) (Download)
25.05.2016 CAT-ACT beamline / XAS data analysis (Download)
08.06.2016 X-ray Microscopy, Surface Analysis by XPS in the Lab & with SR (Download), (Downlaod)
22.06.2016 Time resolved XAS (QEXAFS/DEXAFS) and in situ cell design, spatially resolved XAS, modulation excitation
06.07.2016 Combination of techniques with XAS – part I (IR / Raman Spectroscopy combined with XAS) (Download) (Download)
20.07.2016 Combination of techniques with XAS – part II (XRD, ED-XRD, SAXS) (Downlaod) (Download)