Publikationen der Arbeitsgruppe Prof. Manfred Wilhelm
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Articles 2023 (peer reviewed)
Application of the ramp test from a closed cavity rheometer to obtain the steady-state shear viscosity η (γ̇ ) F. Ellwanger; C. K. Georgantopoulos; H. P. Karbstein; M. Wilhelm; M. Azad Emin; Applied Rheology 33 (2023); DOI 10.1515/arh-2022-0149
Tough PEGgels by In Situ Phase Separation for 4D Printing Z. Wang; M. Heck; W. Yang; M. Wilhelm; P. A. Levkin; Adv Funct Materials; p 2300947 (2023); DOI 10.1002/adfm.202300947
Modeling elongational viscosity of polystyrene Pom-Pom/linear and Pom-Pom/star blends V. Hirschberg; S. Lyu; M. G. Schußmann; M. Wilhelm; M. H. Wagner; Rheol Acta 62; p 433–445 (2023); DOI 10.1007/s00397-023-01411-1
An Intriguing Array of Extrudate Patterns in Long‐Chain Branched Polymers During Extrusion S. Pashazadeh; A. Aulova; C. K. Georgantopoulos; M. Bek; I. Vittorias; I. F. Naue; M. Wilhelm; R. Kádár; Macromol Mater Eng 308 (2023); DOI 10.1002/mame.202300088
Modeling elongational viscosity and brittle fracture of 10 polystyrene Pom-Poms by the hierarchical molecular stress function model V. Hirschberg; M. G. Schußmann; M.-C. Röpert; M. Wilhelm; M. H. Wagner; Rheol Acta; p 269–283 (2023); DOI 10.1007/s00397-023-01393-0
Combined methods for polymer characterization in Rheology and SEC; Kombinierte Methoden zur Polymercharakterisierung in Rheologie und SEC N. Dingenouts; M. Wilhelm; VDI-Berichte; p 645 (engl) 659 (DE) (2023); ISBN 978-3-18-092418-2
From lithium to potassium: Comparison of cations in poly(ethylene oxide)-based block copolymer electrolytes for solid-state alkali metal batteries A. D. Khudyshkina; A. J. Butzelaar; Y. Guo; M. Hoffmann; T. Bergfeldt; M. Schaller; S. Indris; M. Wilhelm; P. Théato; F. Jeschull; Electrochimica Acta 454; p 142421 (2023); DOI 10.1016/j.electacta.2023.142421
Impact of Topological Parameters on Melt Rheological Properties and Foamability of PS POM-POMs M.-C. Röpert; V. Hirschberg; M. G. Schußmann; M. Wilhelm; Macromolecules 56; p 1921–1933 (2023); DOI 10.1021/acs.macromol.2c02051
Molecular Dynamics of Polymyrcene: Rheology and Broadband Dielectric Spectroscopy on a Stockmayer Type A Polymer C. Iacob; M. Heck; M. Wilhelm; Macromolecules 56; 188-197 (2023); DOI 10.1021/acs.macromol.2c01884
Comb and Branch‐on‐Branch Model Polystyrenes with Exceptionally High Strain Hardening Factor SHF > 1000 and Their Impact on Physical Foaming L. Faust; M.-C. Röpert; M. K. Esfahani; M. Abbasi; V. Hirschberg; M. Wilhelm; Macromol. Chem. Phys. 224; p 2200214 (2023); DOI 10.1002/macp.202200214
Role of molecular architecture and temperature on extrusion melt flow instabilities of two industrial LLDPE and LDPE polyethylenes investigated by capillary rheology, high‐pressure sensitivity slit die and optical analysis C. K. Georgantopoulos; M. K. Esfahani; I. F. C. Naue; M. Wilhelm; R. Kádár; J Appl Polym Sci 140; e53165 (2023); DOI 10.1002/app.53165
Complex polymer topologies in blends: Shear and elongational rheology of linear/pom-pom polystyrene blends V. Hirschberg; S. Lyu; M. G. Schußmann; J Rheology 67; p 403–415 (2023); DOI 10.1122/8.0000544
Mechanical fatigue of recycled and virgin high‐/low‐density polyethylene J. Zhang; V. Hirschberg; D. Rodrigue; J Appl Polym Sci 140; p e53312 (2023); DOI 10.1002/app.53312
Further Publications 2023
Spektroskopische Detektion für die Flüssigkeitschromatografie M. Wilhelm; GIT Labor 4; p 14 (2023)
Articles 2022 (peer reviewed)
Threading Polystyrene Stars: Impact of Star to POM‐POM and Barbwire Topology on Melt Rheological and Foaming Properties M.-C. Röpert; A. Goecke; M. Wilhelm; V. Hirschberg; Macromol. Chem. Phys. 223; p 2200288 (2022); DOI 10.1002/macp.202200288
Derivation of a Qualitative Model for the Spatial Characteristic Wavelength of Extrusion Flow Instabilities: Investigation of a Polybutadiene Rubber through Capillary, Slit and Complex Geometry Extrusion Dies C. K. Georgantopoulos; M. K. Esfahani; M. A. Pollard; I. F. C. Naue; A. Causa; R. Kádár; M. Wilhelm; Macromol Mater Eng 300; p 2200313 (2022); DOI 10.1002/mame.202200313
Molecularly Defined Polyolefin Vitrimers from Catalytic Insertion Polymerization L. Odenwald; F. P. Wimmer; N. K. Mast; M. G. Schußmann; M. Wilhelm; S. Mecking; J Am Chem Soc 144; p 13226–13233 (2022); DOI 10.1021/jacs.2c03778
Effect of Side Chain Length in Polystyrene POM–POMs on Melt Rheology and Solid Mechanical Fatigue M.-C. Röpert; M. G. Schußmann; M. K. Esfahani; M. Wilhelm; V. Hirschberg; Macromolecules 55; p 5485–5496 (2022); DOI 10.1021/acs.macromol.2c00199
Sustainable Synthesis of Non‐Isocyanate Polyurethanes Based on Renewable 2,3‐Butanediol A. Kirchberg; M. Khabazian Esfahani; M.-C. Röpert; M. Wilhelm; M. A. R. Meier; Macromol. Chem. Phys. 223; p 2200010 (2022); DOI 10.1002/macp.202200010
Charge Transport and Glassy Dynamics in Blends Based on 1-Butyl-3-vinylbenzylimidazolium Bis(trifluoromethanesulfonyl)imide Ionic Liquid and the Corresponding Polymer M. Hoffmann; C. Iacob; G. Kaysan; M. Simmler; H. Nirschl; G. Guthausen; M. Wilhelm; Polymers (Basel) 14; p 2423 (2022); DOI 10.3390/polym14122423
A new slit‐radial die for simultaneously measuring steady state shear viscosity and first normal stress difference of viscoelastic liquids via capillary rheometry M. Khabazian Esfahani; C. K. Georgantopoulos; I. F. C. Naue; J. Sunder; M. Wilhelm; J Appl Polym Sci 139; p 52094 (2022); DOI 10.1002/app.52094
A Chemometric Approach to Assess the Rheological Properties of Durum Wheat Dough by Indirect FTIR Measurements F. Fanari; G. Carboni; F. Desogus; M. Grosso; M. Wilhelm; Food Bioprocess Technol 15; p 1040–1054 (2022); DOI 10.1007/s11947-022-02799-z
Broadband Dielectric Spectroscopy (BDS) investigation of molecular relaxations in durum wheat dough at low temperatures and their relationship with rheological properties F. Fanari; C. Iacob; G. Carboni; F. Desogus; M. Grosso; M. Wilhelm; LWT 161; p 113345 (2022); DOI 10.1016/j.lwt.2022.113345
Ionogels as Polymer Electrolytes for Lithium–Metal Batteries: Comparison of Poly(ethylene glycol) Diacrylate and an Imidazolium-Based Ionic Liquid Crosslinker M. Hoffmann; A. J. Butzelaar; C. Iacob; P. Theato; M. Wilhelm; ACS Appl. Polym. Mater. (2022); DOI 10.1021/acsapm.2c00075
Poly(ethylene oxide)-Based Electrolytes for Solid-State Potassium Metal Batteries with a Prussian Blue Positive Electrode A. D. Khudyshkina; P. A. Morozova; A. J. Butzelaar; M. Hoffmann; M. Wilhelm; P. Theato; S. S. Fedotov; F. Jeschull; ACS Appl. Polym. Mater. (2022); DOI 10.1021/acsapm.2c00014
Inverse Vulcanization of Norbornenylsilanes: Soluble Polymers with Controllable Molecular Properties via Siloxane Bonds J. M. Scheiger; M. Hoffmann; P. Falkenstein; Z. Wang; M. Rutschmann; V. W. Scheiger; A. Grimm; K. Urbschat; T. Sengpiel; J. Matysik; M. Wilhelm; P. A. Levkin; P. Theato; Angew Chem Int Ed Engl; p e202114896 (2022); DOI 10.1002/anie.202114896
Fourier transformation liquid chromatography: increasing sensitivity by a factor of 50 M. Matz; C. Botha; T. Beskers; M. Wilhelm; Analyst 147; p 1199-1212 (2022); DOI 10.1039/d1an02298a
Nonlinear Schapery viscoelastic material model for thermoplastic polymers T. Zink; L. Kehrer; V. Hirschberg; M. Wilhelm; T. Böhlke; J Appl Polym Sci 139; p 52028 (2022); DOI 10.1002/app.52028
In Situ RheoNMR Correlation of Polymer Segmental Mobility with Mechanical Properties during Hydrogel Synthesis C. Fengler; J. Keller; K.-F. Ratzsch; M. Wilhelm; Adv Sci 9; e2104231 (2022); DOI 10.1002/advs.202104231
Synthesis of Superabsorbent Poly(vinylamine) Core–Shell Particles Monitored by Time-Domain NMR C. Fengler; S. Spange; M. Sommer; M. Wilhelm; Macromolecules 55; p 349–358 (2022); DOI 10.1021/acs.macromol.1c02008
Influence of surface-modified cellulose nanocrystal on the rheological, thermal and mechanical properties of PLA nanocomposites J. Uribe-Calderón; D. Rodrigue; V. Hirschberg; V. V. Fernández-Escamilla; S. C. Pech-Cohuo; Polym. Bull. (2022); DOI 10.1007/s00289-022-04556-w
Mechanical fatigue of biodegradable polymers: A study on polylactic acid (PLA), polybutylene succinate (PBS) and polybutylene adipate terephthalate (PBAT) J. Zhang; V. Hirschberg; D. Rodrigue; International Journal of Fatigue 159; p 106798 (2022); DOI 10.1016/j.ijfatigue.2022.106798
Further Publications 2022
Benchtop‐NMR‐Spektrometer als HPLC‐Detektor Lebensmittelchemie 76; p 212–215 (2022); DOI 10.1002/lemi.202200603
Chemical-sensitive detection in HPLC Botha, C.; Matz, M. u. Wilhelm, M.; Wiley Analytical Science /Hrsg. (2022): https://analyticalscience.wiley.com/do/10.1002/was.001900022
A passion for polymers. Wiley Analytical Science Profile of M. Wilhelm Wilhelm, M. u. Pool, R.; Wiley Analytical Science /Hrsg. (2022): https://analyticalscience.wiley.com/do/10.1002/was.001900022
Articles 2021
Simultaneously monitored quantification of crystallinity and rheological properties of coconut fat via a unique and novel in situ combination of Rheology and 1H NMR technique M. B. Özen; K.-F. Ratzsch; M. Wilhelm; Bulletin of the British Society of Rheology 62; p 75 (2021)
Nanoscopic insight into acrylic acid gelation using low-field RheoNMR C. Fengler; J. Keller; K.-F. Ratzsch; M. Wilhelm; Annual Transactions of the Nordic Rheology Society 29; p 81–86 (2021)
Advanced Block Copolymer Design for Polymer Electrolytes. Prospects of Microphase Separation A. J. Butzelaar; P. Röring; M. Hoffmann; J. Atik; E. Paillard; M. Wilhelm; M. Winter; G. Brunklaus; P. Theato; Macromolecules 54; p 11101–11112 (2021); DOI 10.1021/acs.macromol.1c02147
Nonlinear mechanical behavior of elastomers under tension/tension fatigue deformation as determined by Fourier transform V. Hirschberg; S. Lyu; M. Wilhelm; D. Rodrigue; Rheol Acta 60; p 787–801 (2021); DOI 10.1007/s00397-021-01310-3
One‐Pot Synthesis of Alternating (Ultra‐High Molecular Weight) Multiblock Copolymers via a Combination of Anionic Polymerization and Polycondensation M. Heck; C. Botha; M. Wilhelm; V. Hirschberg; Macromol Rap Commun 41; p 2100448 (2021); DOI 10.1002/marc.202100448
Modeling the spatial characteristics of extrusion flow instabilities for styrene-butadiene rubbers. Investigating the influence of molecular weight distribution, molecular architecture, and temperature C. K. Georgantopoulos; M. K. Esfahani; C. Botha; M. A. Pollard; I. F. C. Naue; A. Causa; R. Kádár; M. Wilhelm; Phys Fluids 33; p 93108 (2021); DOI 10.1063/5.0061334
Styrene-Based Poly(ethylene oxide) Side-Chain Block Copolymers as Solid Polymer Electrolytes for High-Voltage Lithium-Metal Batteries A. J. Butzelaar; P. Röring; T. P. Mach; M. Hoffmann; F. Jeschull; M. Wilhelm; M. Winter; G. Brunklaus; P. Théato; ACS Appl. Mater. Interfaces 13; p 39257–39270 (2021); DOI 10.1021/acsami.1c08841
Universal Strain‐Life Curve Exponents for Thermoplastics and Elastomers under Tension‐Tension and Torsion V. Hirschberg; L. Faust; M. Wilhelm; D. Rodrigue; Macromol Mater Eng 306; p 2100165 (2021); DOI 10.1002/mame.202100165
Rheo-IR: A combined setup for correlating chemical changes via FTIR spectroscopy and rheological properties in a strain-controlled rheometer N. W. Radebe; C. Fengler; C. O. Klein; R. Figuli; M. Wilhelm; J Rheology 65; p 681–693 (2021); DOI 10.1122/8.0000251
Correlation between Macroscopic Elasticity and Chain Dynamics of Natural Rubber during Vulcanization as Determined by a Unique Rheo-NMR Combination S. Nie; K.-F. Ratzsch; S. L. Grage; J. Keller; A. S. Ulrich; J. Lacayo-Pineda; M. Wilhelm; Macromolecules 54; p 6090–6100 (2021); DOI 10.1021/acs.macromol.1c00354
Impact of Water and Flour Components in Dough Investigated Through Low-field Nuclear Magnetic Resonance F. Fanari; J. Keller; F. Desogus; M. Grosso; M. Wilhelm; Chemical Engineering Transactions 87; p 289–294 (2021); DOI 10.3303/CET2187049
Durum Wheat Dough Torque Measurements. Characterization and Study of the Mixing Process Parameters as a Function of Water and Salt Amounts F. Fanari; I. F.C. Naue; F. Desogus; M. Grosso; M. Wilhelm; Chemical Engineering Transactions 87; p 205–210 (2021); DOI 10.3303/CET2187035
Rheo-NMR to investigate fat crystallization under shear F. Rebry; A. Declerck; K.-F. Ratzsch; M. Wilhelm; K. Dewettinck; P. van der Meeren; Current Research in Food Science 4; p 414–420 (2021); DOI 10.1016/j.crfs.2021.05.004
Mechano‐Optical Characterization of Extrusion Flow Instabilities in Styrene‐Butadiene Rubbers. Investigating the Influence of Molecular Properties and Die Geometry C. K. Georgantopoulos; M. K. Esfahani; C. Botha; I. F. C. Naue; N. Dingenouts; A. Causa; R. Kádár; M. Wilhelm; Macromol Mater Eng 306; p 2000801 (2021); DOI 10.1002/mame.202000801
Combining mechanical and thermal surface fourier transform analysis to follow the dynamic fatigue behavior of polymers V. Hirschberg; M. Wilhelm; D. Rodrigue; Poly Test 96; p 107070 (2021); DOI 10.1016/j.polymertesting.2021.107070
Fourier transform fatigue analysis of the stress in tension/tension of HDPE and PA6 V. Hirschberg; M. Wilhelm; D. Rodrigue; Polym Eng Sci 61; p 993–1006 (2021); DOI 10.1002/pen.25616
Reversible and Stable Hemiaminal Hydrogels from Polyvinylamine and Highly Reactive and Selective Bis(N -acylpiperidone)s T. Uhlig; C. Fengler; A. Seifert; F. Taubert; L. Kaßner; H.-J. Hähnle; C. Hamers; M. Wilhelm; S. Spange; M. Sommer; ACS Macro Lett. 10; p 389–394 (2021); DOI 10.1021/acsmacrolett.0c00904
Solvent suppression techniques for coupling of size exclusion chromatography and 1H NMR using benchtop spectrometers at 43 and 62 MHz J. Höpfner; B. Mayerhöfer; C. Botha; D. Bouillaud; J. Farjon; P. Giraudeau; M. Wilhelm; Journal of Magnetic Resonance 323; p 106889 (2021); DOI 10.1016/j.jmr.2020.106889
Dual-faced borax mediated synthesis of self-healable hydrogels merging dynamic covalent bonding and micellization X. Li; H. Mutlu; C. Fengler; M. Wilhelm; P. Theato; Polym Chem 12; p 361–369 (2021); DOI 10.1039/D0PY01354D
Investigation of the Porosity of Poly(sodium methacrylate) Hydrogels by 1 H‐NMR T2 ‐Relaxation and Inverse Size‐Exclusion Chromatography C. Pfeifer; F. Cavalli; B. Huber; P. Theato; L. Barner; M. Wilhelm; Macromol. Chem. Phys. 222; p 2000300 (2021); DOI 10.1002/macp.202000300
Quantifying separation energy with a modified Capillary Break-up Extensional Rheometer (CaBER) to study polymer solutions K. Riazi; M. Abbasi; C. O. Klein; I. F. C. Naue; M. Wilhelm; Soft Materials 19; p 199–200 (2021); DOI 10.1080/1539445X.2020.1792929
Articles 2020
Desalination of Seawater Using Cationic Poly(acrylamide) Hydrogels and Mechanical Forces for Separation C. Fengler; L. Arens; H. Horn; M. Wilhelm; Macromol Mater Eng 305; p 2000383 (2020); DOI 10.1002/mame.202000383
Interlaboratory study on rheological properties of cement pastes and reference substances. Comparability of measurements performed with different rheometers and measurement geometries M. Haist; J. Link; D. Nicia; S. Leinitz; C. Baumert; T. von Bronk; D. Cotardo; M. Eslami Pirharati; S. Fataei; H. Garrecht; C. Gehlen; I. Hauschildt; I. Ivanova; S. Jesinghausen; C. Klein; H.-W. Krauss; L. Lohaus; D. Lowke; O. Mazanec; S. Pawelczyk; U. Pott; N. W. Radebe; J. J. Riedmiller; H.-J. Schmid; W. Schmidt; E. Secrieru; D. Stephan; M. Thiedeitz; M. Wilhelm; V. Mechtcherine; Mater Struct 53; p 63 (2020); DOI 10.1617/s11527-020-01477-w
Optimizing the Power Production in an Osmotic Engine via Microfluidic Fabricated and Surface Crosslinked Hydrogels Utilizing Fresh and Salt Water A. Jangizehi; C. Fengler; L. Arens; M. Wilhelm; Macromol Mater Eng 305; p 2000174 (2020); DOI 10.1002/mame.202000174
Effect of Topology and Molecular Properties on the Rheology and Fatigue Behavior of Solid Polystyrene/Polyisoprene Di- and Triblock Copolymers V. Hirschberg; L. Faust; D. Rodrigue; M. Wilhelm; Macromolecules 53; p 5572–5587 (2020); DOI 10.1021/acs.macromol.0c00632
Rheological and mechanical properties of cellulose/LDPE composites using sustainable and fully renewable compatibilisers P. B. V. Scholten; M. B. Özen; Z. Söyler; J.‐M. Thomassin; M. Wilhelm; C. Detrembleur; M. A. R. Meier; J Appl Polym Sci 137; p 48744 (2020); DOI 10.1002/app.48744
Molecular origin of the foam structure in model linear and comb polystyrenes. II. Volume expansion ratio M. Abbasi; L. Faust; M. Wilhelm; Polymer 193; p 122354 (2020); DOI 10.1016/j.polymer.2020.122354
Molecular origin of the foam structure in model linear and comb polystyrenes. I. Cell density M. Abbasi; L. Faust; M. Wilhelm; Polymer 193; p 122351 (2020); DOI 10.1016/j.polymer.2020.122351
Gradient-Induced Mechanical Vibration of Neural Interfaces During MRI I.E. Fuhrer; M. Jouda; C. O. Klein; M. Wilhelm; J. G. Korvink; IEEE Trans Biomed Eng 67; p 915–923 (2020); DOI 10.1109/TBME.2019.2923693
Small and Medium Amplitude Oscillatory Shear Rheology of Model Branched Polystyrene (PS) Melts H. Y. Song; L. Faust; J. Son; M. Kim; S. J. Park; S.-K. Ahn; M. Wilhelm; K. Hyun; Polymers (Basel) 12 (2020); DOI 10.3390/polym12020365
Cumulative nonlinearity as a parameter to quantify mechanical fatigue V. Hirschberg; M. Wilhelm; D. Rodrigue; Fatigue Fract Eng Mater Struct 43; p 265–276 (2020); DOI 10.1111/ffe.13120
Dynamic rheology and mechanics of polymers in their solid state V. Hirschberg; M. Wilhelm; D. Rodrigue. In: Thomas, S.; Chandrasekharakurup, S. u. Chandran, N. (Eds.); Rheology of Polymer Blends and Nanocomposites. Theory, Modelling and Applications. Elsevier. San Diego (2020); DOI 10.1016/B978-0-12-816957-5.00012-4, ISBN 9780128169568; p 241-161.
Chondroinductive Alginate-Based Hydrogels Having Graphene Oxide for 3D Printed Scaffold Fabrication F. Olate-Moya; L. Arens; M. Wilhelm; M. A. Mateos-Timoneda; E. Engel; H. Palza; ACS Appl Mater Interfaces 12; p 4343–4357 (2020); DOI 10.1021/acsami.9b22062
Analysis of the Local Mobility of RAFT Mediated Poly(acrylic acid) Networks via Low Field 1 H‐NMR Techniques for Investigation of the Network Topology F. Cavalli; C. Pfeifer; L. Arens; L. Barner; M. Wilhelm; Macromol. Chem. Phys. 221; p 1900387 (2020); DOI 10.1002/macp.201900387
Effect of Different Molecular Weights and Chemical Composition of Superplasticizers on the Structural Build-up of Cement Paste Using Dynamic Oscillatory Rheology N. W. Radebe; C. O. Klein. In: Boshoff, W. P.; Combrinck, R. u. Mechtcherine, V. (Eds.); 3rd International Conference on the Application of Superabsorbent Polymers (SAP) and Other New Admixtures Towards Smart Concrete. SAP 2019, Rilem (2020); DOI 10.1007/978-3-030-33342-3_21; ISBN 9783030333423; p 192–199
Use of Combined Rheo-NMR to Investigate the Relationship Between the Molecular and Mechanical Properties of Early Cement Paste Hydration N. W. Radebe; K.-F. Ratzsch; C. O. Klein; M. Wilhelm. In: Mechtcherine, V.; Khayat, K. u. Secrieru, E. (Eds.); Rheology and Processing of Construction Materials. RheoCon2 et SCC9. Springer. Cham, Switzerland (2020); DOI 10.1007/978-3-030-22566-7_30; ISBN 3030225666; p 256–265.
Articles 2019
Poly(sodium acrylate) hydrogels. Synthesis of various network architectures, local molecular dynamics, salt partitioning, desalination and simulation L. Arens; D. Barther; J. Landsgesell; C. Holm; M. Wilhelm; Soft Matter 15; p 9949–9964 (2019); DOI 10.1039/c9sm01468c
Erkenntnisgewinn durch Systemanalyse und Testing – Ein Ansatz zur Unterstützung der Entwicklung von Systemen mit neuartigen Wirkprinzipien. Gain of insights through system analysis and testing – an approach to support development of systems with new working principle S. Matthiesen; M. Wilhelm; P. Grauberger; I. F. C. Naue; Stuttgarter Symposium für Produktentwicklung SSP 2019 : Stuttgart, 16. Mai 2019, Wissenschaftliche Konferenz (2019).  DOI 10.18419/opus-10394
Self‐Assembled Acrylic ABA Triblock Copolymer Hydrogels with Various Block Compositions. Water Absorbency, Rheology, and SAXS L. Arens; M. Wilhelm; Macromol. Chem. Phys. 220, 1900093 (2019); DOI 10.1002/macp.201900093
Investigation of Melt Flow Instabilities in SBR: Influence of MWD and Microstructure at In Situ Pressure Fluctuations as Detected by Capillary Rheology C. K. Georgantopoulus; I. F. C. Naue; A. Causa; L. Garro; M. Wilhelm; Ann. Trans. Nordic Rheology Soc. 27, 151-158 (2019)  File
Aging of natural rubber studied via Fourier-transform rheology and double quantum NMR to correlate local chain dynamics with macroscopic mechanical response S. Nie; J. Lacayo-Pineda; N. Willenbacher; M. Wilhelm; Polymer 181; p 121804 (2019); DOI 10.1016/j.polymer.2019.121804
Fatigue analysis of brittle polymers via Fourier transform of the stress V. Hirschberg; F. Lacroix; M. Wilhelm; D. Rodrigue; Mech. Mat. 137, 103100 (2019); DOI 10.1016/j.mechmat.2019.103100
1H PFG‐NMR Diffusion Study on a Sequence‐Defined Macromolecule. Confirming Monodispersity X. Guo; K. S. Wetzel; S. C. Solleder; S. Spann; M. A. R. Meier; M. Wilhelm; B. Luy; G. Guthausen; Macromol. Chem. Phys. 220, 1900155 (2019); DOI 10.1002/macp.201900155
A New Quantum Cascade IR-Laser Online Detector. Chemical-Sensitive Size-Exclusion Chromatography Measurement at Unprecedented Low Levels J. M. Kübel; C. Botha; A. Bucka; J. Höpfner; H. Zimmermann; M. Godejohann; M. Wilhelm; Macromol Rap Commun 40, e1900228 (2019); DOI 10.1002/marc.201900228
Fourier-transform rheology of unvulcanized styrene butadiene rubber filled with increasingly silanized silica S. Nie; J. Lacayo-Pineda; M. Wilhelm; Soft Materials 17, 269-282 (2019); DOI 10.1080/1539445X.2018.1542314
Comb and Bottlebrush Polymers with Superior Rheological and Mechanical Properties M. Abbasi; L. Faust; M. Wilhelm; Adv. Mater. 31, 1806484 (2019); DOI 10.1002/adma.201806484
Structure of Superabsorbent Polyacrylate Hydrogels and Dynamics of Counterions by Nuclear Magnetic Resonance X. Guo; C. Pfeifer; M. Wilhelm; B. Luy; G. Guthausen; Macromol. Chem. Phys. 220, 1800525 (2019); DOI 10.1002/macp.201800525
On-line SEC-MR-NMR hyphenation. Optimization of sensitivity and selectivity on a 62 MHz benchtop NMR spectrometer

C. Botha; J. Höpfner; B. Mayerhöfer; M. Wilhelm; Polym. Chem. 10, 2230–2246 (2019); DOI 10.1039/C9PY00140A

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Interfacial Fourier Transform Shear Rheometry of Complex Fluid Interfaces C. O. Klein; A. Theodoratou; P. A. Rühs; U. Jonas; B. Loppinet; M. Wilhelm; P. Fischer; J. Vermant; D. Vlassopoulos; Rheol. Acta 58, 29–45 (2019); DOI 10.1007/s00397-018-01122-y
Polymer Crystallization Studied by Hyphenated Rheology Techniques. Rheo‐NMR, Rheo‐SAXS, and Rheo‐Microscopy

V. Räntzsch; M. B. Özen; K.‐F. Ratzsch; E. Stellamanns; M. Sprung; G. Guthausen; M. Wilhelm; Macromol. Mater. Eng. 304, 1800586 (2019); DOI 10.1002/mame.201800586

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Comb Polymers with Triazole Linkages under Thermal and Mechanical Stress C. Petit; M. Abbasi; T. S. Fischer; M. Wilhelm; A. S. Goldmann; C. Barner-Kowollik; Macromolecules 52, 420–431 (2019); DOI 10.1021/acs.macromol.8b02174
Dynamics of Sodium Ions and Water in Swollen Superabsorbent Hydrogels as Studied by 23 Na- and 1 H-NMR X. Guo; S. Theissen; J. Claussen; V. Hildebrand; J. Kamphus; M. Wilhelm; B. Luy; G. Guthausen; Macromolecular Chemistry and Physics 220, 1800350 (2019); DOI 10.1002/macp.201800350
Articles 2018
Investigation on Rubber Cross-linking via Rheo-NMR: Microscopic Chain Dynamic and Macroscopic Rheological Response S. Nie; K.-F. Ratzsch; V. Räntzsch; M. Wilhelm; J. Lacayo-Pineda; 13th Fall Rubber Colloquium (2018); ISBN 9783981407631.
Medium Resolution 1H-NMR at 62 MHz as a chemical sensitive Online Detector for Size Exclusion Chromatography (SEC-NMR) C. Botha; J. Höpfner; B. Mayerhöfer; M. Wilhelm; 13th Fall Rubber Colloquium, 118 (2018); ISBN 9783981407631.
High sensitivity measurements of normal force under large amplitude oscillatory shear I. F. C. Naue; R. Kádár; M. Wilhelm; Rheologica Acta 57, 757–770 (2018); DOI 10.1007/s00397-018-1111-y
Poly(propylene-co-1-pentene-co-1-heptene) terpolymers. Mechanical and rheological behavior A. García-Peñas; J. M. Gómez-Elvira; V. Lorenzo; M. Wilhelm; E. Pérez; M. L. Cerrada; Polymer 156, 44–53 (2018); DOI 10.1016/j.polymer.2018.09.057
A novel 3D printed mechanical actuator using centrifugal force for magnetic resonance elastography. Initial results in an anthropomorphic prostate phantom W. Neumann; A. Bichert; J. Fleischhauer; A. Stern; R. Figuli; M. Wilhelm; L. R. Schad; F. G. Zöllner; PloS one 13, e0205442 (2018); DOI 10.1371/journal.pone.0205442
Nonlinear Oscillatory Shear Mechanical Responses K. Hyun; M. Wilhelm. In: Richert, R. (Ed.); Nonlinear Dielectric Spectroscopy. Advances in Dielectrics (2018); DOI 10.1007/978-3-319-77574-6_11
Stability of Diels–Alder photoadducts in macromolecules C. Petit; L. D. Bangert; M. Abbasi; M. Wilhelm; A. S. Goldmann; C. Barner-Kowollik; Polymer Chemistry 9, 3850–3854 (2018); DOI 10.1039/C8PY00748A
Transitions between Lamellar Orientations in Shear Flow L. Schneider; M. Heck; M. Wilhelm; M. Müller; Macromolecules 51, 4642–4659 (2018); DOI 10.1021/acs.macromol.8b00825
Influence of molecular structure on the foamability of polypropylene: A rheological fingerprint E. Bahreini, S. F. Aghamiri, M. Wilhelm, M. Abbasi; J. Cell. Plast. 54 515-543 (2018); DOI: 10.1177/0021955X17700097
Polymer crystallinity and crystallization kinetics via benchtop 1H-NMR relaxometry. Revisited method, data analysis, and experiments on common polymers V. Räntzsch; M. Haas; M. B. Özen; K.-F. Ratzsch; K. Riazi; S. Kauffmann-Weiss; J. K. Palacios; A. J. Müller; I. Vittorias; G. Guthausen; M. Wilhelm; Polymer 145, 162–173 (2018); DOI 10.1016/j.polymer.2018.04.066
Fatigue life prediction via the time-dependent evolution of linear and nonlinear mechanical parameters determined via Fourier transform of the stress V. Hirschberg; M. Wilhelm; D. Rodrigue; Journal of Applied Polymer Science 135, 46634 (2018); DOI 10.1002/app.46634
Topological Insight into Superabsorbent Hydrogel Network Structures. A 1 H Double-Quantum NMR Study X. Guo; S. Theissen; J. Claussen; V. Hildebrand; J. Kamphus; M. Wilhelm; B. Luy; G. Guthausen; Macromolecular Chemistry and Physics 219, 1800100 (2018); DOI 10.1002/macp.201800100
Padé approximant for normal stress differences in large-amplitude oscillatory shear flow P. Poungthong; C. Saengow; A. J. Giacomin; C. Kolitawong; D. Merger; M. Wilhelm; Physics of Fluids 30, 40910 (2018); DOI 10.1063/1.5013203
Diblock Copolymers with Similar Glass Transition Temperatures in Both Blocks for Comparing Shear Orientation Processes with DPD Computer Simulations M. Heck; L. Schneider; M. Müller; M. Wilhelm; Macromolecular Chemistry and Physics 219, 1700559 (2018); DOI 10.1002/macp.201700559
Influence of molecular properties on the mechanical fatigue of polystyrene (PS) analyzed via Wöhler curves and Fourier Transform rheology V. Hirschberg; L. Schwab; M. Cziep; M. Wilhelm; D. Rodrigue; Polymer 138 1–7 (2018); DOI:10.1016/j.polymer.2018.01.042
Medium resolution 1H-NMR at 62 MHz as a new chemically sensitive online detector for size exclusion chromatography (SEC-NMR) J. Höpfner, K.F. Ratzsch, C. Botha, M. Wilhelm; Macromol. Rapid Commun. 39 1700766 (2018); DOI: 10.1002/marc.201700766
Experimental investigation of the permeability of a tribo-Contact in the dry friction clutches H. Clausnizer, A. Fidlin, R. Figuli, G. Jehle, M. Wilhelm, J.S. Keller; Tribology Int. 118 157-162 (2018); DOI:10.1016/j.triboint.2017.09.031
Online Detection of Functional groups in SEC via Quantum Cascade Laser IR Spectroscopy S. Morlock, J.M. Kübel, T.F. Beskers, B. Lendl, M. Wilhelm; Macromol. Rapid Commun. 39, 1700307 (2018); DOI: 10.1002/marc.201700307
Articles 2017
Low-field RheoNMR: Newly developed combination of rheology and time domain (TD)-NMR to correlate mechanical properties with molecular dynamics in polymer melts V. Räntzsch, M.B. Özen, K.-F. Ratzsch, G. Guthausen, M. Wilhelm; PPS-32: 32nd Int. Conference of the Polymer Processing Society; AIP Conference Proceedings 1914, 110001 (2017); DOI: 10.1063/1.5016756
Energy consumption for the desalination of salt water using polyelectrolyte hydrogels as the separation agent L. Arens, J.B. Albrecht, J. Höpfner, K. Schlag, M. Wilhelm; Macromol. Chem. Phys. 218 1700237 (2017); DOI: 10.1002/macp.201700237
Analysis of the reaction behavior of highly concentrated plant proteins in extrusion-like conditions M. Azad Emin, M. Quevedo, M. Wilhelm, H.P. Karbstein; Innovative Food Science and Emerging Technologies 44 15-20 (2017); DOI: 10.1016/j.ifset.2017.09.013
Dynamic Rheology and Mechanics of Polymers in their Solid State V. Hirschberg; M. Wilhelm; D. Rodrigue. In: Rivera-Armenta, J. L. (Ed.); Polymer Rheology. INTECHOPEN (2017)
The Intrinsic Mechanical Nonlinearity 3Q0(ω) of Linear Homopolymer Melts M.A. Cziep, M. Abbasi, M. Wilhelm; Novel Trends in Rheology VII, AIP Conference Proceedings 1843 0400002 (2017) ISBN 978-0-7354-1513-3; DOI: 10.1063/1.4982991
Shear Rheology and 1H TD-NMR Combined to Low-Field RheoNMR: Set-Up and Application to Quiescent and Flow-Induced Crystallization of Polymers V. Räntzsch, M.B. Özen, K.-F. Ratzsch, G. Guthausen, M. Wilhelm; Novel Trends in Rheology VII, AIP Conference Proceedings 1843 0400001 (2017) ISBN 978-0-7354-1513-3; DOI: 10.1063/1.4982990
Linear and Extensional Rheology of Model Branched Polystyrenes: from Loosly-grafted Combs to Bottlebrushes M. Abbasi, L. Faust, K. Riazi, M. Wilhelm; Macromolecules 50 5964-5977 (2017); DOI: 10.1021/acs.macromol.7b01034
KIT: Abteilung „Polymere Materialien“ am Institut für Technische Chemie und Polymerchemie N. Dingenouts, Ch. Klein, M. Wilhelm; GAK Gummi Fasern Kunststoffe 70 360-361 (2017)
Low-field rheo-NMR: A novel combination of NMR relaxometry with high end shear rheology K.F. Ratzsch, Ch. Friedrich, M. Wilhelm; J. Rheol. 61 905-917 (2017); DOI: 10.1122/1.4991513
Low-field Rheo-NMR: A portable 1H TD-NMR unit for shear rheometers and its application to quiescent and flow induced crystallization of polyolefines V. Räntzsch, B.M. Özen, K.F. Ratzsch, G. Guthausen, M. Wilhelm; 30th International Symposium on Polymer Analysis and Characterisation (ISPAC) 2017; ISBN978-3-99062-106-6, p. 19
Osmotic Engine: Translating Osmotic Pressure into Macroscopic Mechanical Force via Poly(Acrylic Acid) Based Hydrogels L. Arens, F. Weißenfeld, C.O. Klein, K. Schlag, M. Wilhelm; Advanced Science 1700112 (2017); DOI: 10.1002/advs.201700112
Link to full article containing title page
Fatigue Behavior of Polystyrene (PS) analyzed from the Fourier Transform (FT) of its Stress Response: First evidence of I2/1(N) and I3/1(N) as new fingerprints V. Hirschberg, M. Wilhelm, D. Rodrigue; Polymer Testing 60 343-350 (2017); DOI: 10.1016/j.polymertesting.2017.04.001
Diffusion in Polymer Solutions: Molecular Weight Distribution by PFG-NMR and Relation to SEC X. Guo, E. Laryea, M. Wilhelm, B. Luy, H. Nirschl, G. Guthausen; Macromol. Chem. Phys. 218 DOI: 10.1002/macp.201600440
Linear and nonlinear rheology combined with dielectric spectroscopy of hybrid polymer nanocomposites for semiconductive applications R. Kádár, M. Abbasi, R. Figuli, M. Rigdahl, M. Wilhelm; Nanomaterials 7 23 (2017); DOI: 10.3390/nano7020023
Articles 2016
Divergence of third harmonic stress response to oscillatory strain approaching the glass transition R. Seyboldt, D. Merger, F. Coupette, M. Siebenbürger, M. Ballauff, M. Wilhelm, M. Fuchs; Soft Matter 12, 8825-8832 (2016); DOI: 10.1039/c6sm01616b
Simultaneous analysis: In situ and concurrent dielectric and dynamic mechanical thermal analysis H. Deckmann, R. Figuli, M. Wilhelm, H. Mucha, J. Lacayo, M. Wilhelm; Tire Technology International 2016, 72-73 (2016)
Determination of physical emulsion stabilization mechanisms of wood hemicelluloses via rheological and interfacial characterization K.S. Mikkonen, D. Merger, P. Kilpeläinen, L. Murtomäki, U.S. Schmidt, M. Wilhelm; Soft Matter 12, 8690-8700 (2016); DOI 10.1039/C6SM01557C
Simple scalar model for Large Amplitude Oscillatory Shear D. Merger, M. Abbasi, J. Merger, A.J. Giacomin, Ch. Saengow, M. Wilhelm; Appl. Rheol. 26, 53809 (2016); DOI 10.3933/ApplRheol-26-53809
Polystyrene comb architectures as model systems for the optimized solution electrospinning of branched polymers K. Riazi, J. Kübel, M. Abbasi, K. Bachtin, S. Indris, H. Ehrenberg, R. Kádár, M. Wilhelm; Polymer 104, 240-250 (2016); DOI 10.1016/j.polymer.2016.05.032
First normal stress difference and in-situ spectral dynamics in a high sensitivity extrusion die for capillary rheometry via the ’hole effect’ R. Kádár, I.F.C. Naue, M. Wilhelm; Polymer 104, 193-203 (2016); DOI 10.1016/j.polymer.2016.07.061
Special issue on “Polymer rheology” (Editorial) M. H. Wagner, M. Wilhelm; Polymer 104, 170 (2016) DOI 10.1016/j.polymer.2016.05.054
Newly Developed Combination of Rheology and 1H TD-NMR to Correlate Mechanical Properties with Moleculare Dynamics in Soft Matter M. B. Özen, V. Räntzsch, K.-Ratzsch, G. Guthausen, M. Wilhelm; Annual Transactions of the Nordic Rheology Society 24, 33-39 (2016), ISBN 978-91-637-9105-5
Influence of processing conditions on the linear and non-linear oscillatory shear, extensional and combined dielectric –rheological properties of poly(ethylene-buthylacrylate) – graphite nanoplatelets – carbon black hybrid nanocomposites R. R. Kádár, M. Abbasi, R. Figuli, R. Arino, M. Rigdahl, M. Wilhelm; Annual Transactions the Nordic Rheology Society 24, 23-24 (2016), ISBN 978-91-637-9105-5
Effect of molecular weight, polydispersity and monomer of linear homopolymer melts on the intrinsic mechanical nonlinearity 3Qo(w) in MAOS M.A. Cziep, M. Abbasi, M. Wilhelm; Annual Transactions of the Nordic Rheology Society 24, 9-13 (2016), ISBN 978-91-637-9105-5
Rheological Characterization of Thermoplastic Elastomers (TPE) Based on PP and Recycled EPDM P. Mahallati, H. M. Hassanabadi, M. Wilhelm, D. Rodrigue;  Appl. Rheol. 26 33503 (2016), DOI 10.3933/ApplRheol-26-33503
Bestimmung der inneren Oberfläche in rußgefülltem SBR mit Hilfe der FT-Rheologie L. Schwab, N. Hojdis, J. Lacayo, M. Wilhelm; Gummi, Fasern, Kunststoffe 69 358-364 (2016)
Hyphenated low-field NMR techniques: combining NMR with NIR, GPC/SEC and rheometry V. Räntzsch, M. Wilhelm, G. Guthausen; Magn. Reson. Chem. 54, 494–501 (2016); DOI 10.1002/mrc.4219
Effect of Molecular Weight, Polydispersity and Monomer of Linear Homopolymer Melts on the Intrinsic Mechanical Nonlinearity 3Q0(w) in MAOS M.A. Cziep, M. Abbasi, M. Heck, L. Arens, M. Wilhelm; Macromolecules 49, 3566−3579 (2016); DOI: 10.1021/acs.macromol.5b02706
Fourier–Transform rheology of unvulcanized, carbon black filled styrene butadiene rubber L. Schwab, N. Hojdis, J. Lacayo-Pineda, M. Wilhelm; Macromol. Mat. Eng. 301 457-468 (2016); DOI: 10.1002/mame.201500356
Combined Dielectric (DEA) and Dynamic Mechanical Thermal Analysis (DMTA) in compression mode R. Figuli, L. Schwab, J. Lacayo-Pineda, H. Deckmann, M. Wilhelm; Kautsch. Gummi Kunstst. 69 22-27 (2016)
Effect of Carbon-Based Particles on the Mechanical Behavior of Isotactic Polypropylenes C. Garzóna, M. Wilhelm, M. Abbasi, H. Palza; Macromol. Mater. Eng. 301 429-440 (2016); DOI: 10.1002/mame.201500380
Articles 2015
A New High Sensitivity System to Detect Instabilities During the Extrusion of Polymer Melts I.F.C. Naue, R. Kádár, M. Wilhelm; Macromol. Mater. Eng. 300 1141–1152 (2015); DOI: 10.1002/mame.201500148
Ready access to end-functional polystyrenes via a combination of ARGET ATRP and thiol–ene chemistry O. Altintas; T. Josse, J. De Winter, N.M. Matsumoto, P. Gerbaux, M. Wilhelm, C. Barner-Kowollik; Polym. Chem. 6 6897–7072 (2015); DOI: 10.1039/c5py01048a
Large amplitude oscillatory shear applications for the characterization of dispersed systems D. Merger, K. Reinheimer, M. Grosso, J.M. Brader, M. Ballauff, J. Kim, M.E. Helgeson, M. Wilhelm; in M. Kind et al. (eds.) "Colloid Process Engineering”, Springer Verlag (2015); DOI 10.1007/978-3-319-15129-8_6
Correlating crystallization kinetics and rheological properties of polyethylene using a new Rheo-NMR setup B. Özen, F. Ratzsch, V. Räntzsch, M. Wilhelm; 4th International Polymeric Composites Symposium, Izmir, Türkei; ISBN 978-605-01-0724-1; S. 337
Non-linear rheology and combined methods in rheology and processing M. Wilhelm; 4th International Polymeric Composites Symposium, Izmir, Türkei; ISBN 978-605-01-0724-1; S. 154
Living Radical Polymers under Melt processing conditions Ö. Altintas, C. Barner-Kowollik, M. Wilhelm; 4th International Polymeric Composites Symposium, Izmir, Türkei; ISBN 978-605-01-0724-1; S. 33
Online coupling of specialty detectors in GPC for chemical and molar mass detection J.A. McConville, D. Lohmann, T. Hofe, M. Cudaj, G. Guthausen, M. Wilhelm; 249th ACS National Meeting & Exposition, Denver, CO, United States, March 22-26, 2015 (2015), POLY-315.
Untersuchung des Kristallisationsverhaltens von Polyolefinen mithilfe einer neuentwickelten Rheo-NMR K.F. Ratzsch, M. Wilhelm; Anwenderseminar TA-Instruments, User Meeting 2014, Würzburg
Fourier-transform Dynamic mechanical thermal analysis - a new tool for the analysis of the thermo-rheological behavior of polymers and polymer sandwich composites R. Kádár, I. Vittorias, M. Wilhelm, A. Mulone; The 15th International Conference on Deformation, Yield and Fracture of Polymers - Book of Abstracts 432-434 (2015)
ATRP-based Polymers with Modular Ligation Points under Thermal and Mechanical Stress O. Altintas; T. Josse, M. Abbasi, J. De Winter, V. Trouillet, P. Gerbaux, M. Wilhelm, C. Barner-Kowollik; Polym. Chem. 6 2854-2868 (2015); DOI: 10.1039/c5py00036j
Large-Amplitude Oscillatory Shear: Comparing Parallel-Disk with Cone-Plate Flow A.J. Giacomin, P.H. Gilbert, D. Merger, M. Wilhelm; Rheol. Acta 54 263-285 (2015); DOI 10.1007/s00397-014-0819-6
Development of a chemically sensitive online SEC detector based on FTIR spectroscopy T. F. Beskers, T. Hofe, M. Wilhelm; Polym. Chem. 6 128-142 (2015); DOI 10.1039/C4PY01043D
Synthesis and small angle X-ray scattering (SAXS) characterization of silica spheres covered with gel-like particles formed by means of solvent evaporation A. Gutsche, X. Guo, N. Dingenouts, H. Nirschl; Powder Technology 278 257–265 (2015); DOI:10.1016/j.powtec.2015.03.037
Articles 2014
Molecular Dynamics of Polymer Composites Using Rheology and Combined RheoNMR ... V. Räntzsch, K.-F. Ratzsch, G. Guthausen, S. Schlabach, M. Wilhelm; Soft Materials 12, 4-13 (2014); DOI 10.1080/1539445X.2014.930045
A rheological criterion to determine the percolation threshold in polymer nano-composites H. M. Hassanabadi, M. Wilhelm, D. Rodrigue; Rheol Acta 53 869–882 (2014); DOI 10.1007/s00397-014-0804-0
IR Spectroscopy as a novel detector for Size Exclusion Chromatography T.F. Beskers, J. Kübel, A. Simon, T. Hofe, M. Wilhelm; KHK 11th Fall Rubber Colloquium (2014), ISBN 978 398 140 7624
Simultaneous In-situ Analysis of Instabilities and First Normal Stress Difference during Polymer Melt Extrusion Flows R. Kádár, I.F.C. Naue, M. Wilhelm; Annual Transaction of the Nordic Rheology Society 22 153-160 (2014)
Network structure and inhomogeneities of model and commercial polyelectrolyte hydrogels as investigated by low-field proton NMR techniques J. Höpfner, G. Guthausen, K. Saalwächter, M. Wilhelm;
Macromolecules 47 4251-4265 (2014); DOI 10.1021/ma500558v
Intrinsic Nonlinearity from LAOStrain - Experiments on various strain and stress-controlled rheometers: A quantitative comparison D. Merger, M. Wilhelm;
Rheol. Acta 53 621-634 (2014) DOI 10.1007/s00397-014-0781-3
Microstructure and nonlinear signatures of yielding in a heterogeneous colloidal gel under large amplitude oscillatory shear  J. Kim, D. Merger, M. Wilhelm, M.E. Helgeson;
 J. Rheol. 58 1319-1390 (2014); DOI: 10.1122/1.4882019
Large Amplitude Oscillatory Shear and Fourier Transform Rheology Analysis of Branched Polymer Melts D. M. Hoyle, D. Auhl, V. Barroso, O. G. Harlen, M. Wilhelm, T. C. M. McLeish; J. Rheol. 58 969-997 (2014); DOI: 10.1122/1.4881467
Application of design of experiments, response surface methodology and partial least squares regression on nanocomposites synthesis V. H. Campos-Requena, B. L. Rivas, M. A. Perez, M. Wilhelm; Polym. Bull. 71 1961-1982 (2014); DOI 10.1007/s00289-014-1166-6
New way to characterize the percolation threshold of polyethylene and carbon nanotube polymer composites using Frourier Transform (FT)-Rheology D. Ahirwal, H. Palza, G. Schlatter, M. Wilhelm;
Korea-Aust. Rheol. J. 26 319-326 (2014); DOI: 10.1007/s13367-014-0036-y
Oscillatory shear and high-pressure dielectric study of 5-methyl-3-heptanol C. Gainaru, M. Wikarek, S. Pawlus, M. Paluch, R. Figuli, M. Wilhelm, T. Hecksher, B. Jakobsen, J. C. Dyre, R. Böhmer; Colloid and Polymer Science 292 1913-1921 (2014);  DOI 10.1007/s00396-014-3274-0
Stability of Star-shaped RAFT Polystyrenes under Mechanical and Thermal Stress O. Altintas, M. Abbasi, K. Riazi, A.S. Goldmann, N. Dingenouts, M. Wilhelm, C. Barner-Kowollik; Polymer Chemistry 5 5009-5019 (2014); DOI 10.1039/C4PY00484A
Large amplitude oscillatory shear and uniaxial extensional rheology of blends from linear and long-chain branched polyethylene and polypropylene D. Ahirwal, S. Filipe, I. Neuhaus, M. Busch, G. Schlatter, M.Wilhelm; J. Rheol. 58 635-658 (2014); DOI 10.1122/1.4867555
Investigation of Polymer-filler Interactions inTiO2-filled Poly(n-alkylmethacrylates) by Low Field NMR Relaxometry G. Guthausen, V. Räntzsch, C. Biquet, S. Schlabach, M. Wilhelm; Macromol. Chem. Phys. 215 851-858 (2014) DOI 10.1002/macp.201400017
Adaptable Hetero Diels–Alder Networks for Fast Self-Healing under Mild Conditions K.K. Oehlenschlaeger, J.O. Mueller, J. Brandt, S. Hilf, A. Lederer, M. Wilhelm, R. Graf, M.L. Coote, F.G. Schmidt, C. Barner-Kowollik; Advanced Materials 26 3561–3566 (2014); DOI 10.1002/adma.201306258
High Performance Liquid Chromatographie with Mid-Infrared Detection based on broadly tunable Quantum Cascade Laser T.F. Beskers, M. Brandstetter, J. Kuligowski, G. Quintás, M. Wilhelm, B. Lendl; Analyst 139 2057-2064 (2014); DOI 10.1039/c3an01546g
Measurement of the frequency dependence of the shear modulus of monohydroxy alcohols: Evidence for a short-chain-polymer rheological response C. Gainaru, R. Figuli, T. Hecksher, B. Jakobsen, J.C. Dyre, M. Wilhelm, R. Böhmer; Phys. Rev. Letters 112 098301 (2014) DOI 10.1103/PhysRevLett.112.098301
Rheology, Electrical Properties, and
Percolation of TRGO-Filled EVA-Copolymers
K.-F. Ratzsch, V. Cecen, F. Tölle, K.-A. Wartig,
R. Thomann, R. Mülhaupt, C. Friedrich; Macromol. Materials Engineering; ahead of print (2014) DOI 10.1002/mame.201300440
Time-resolved SAXS characterization of the shell growth of silica-coated magnetite nanocomposites A. Gutsche, A. Daikeler, X. Guo, N. Dingenouts, H. Nirschl; J Nanopart Res 16 2475 (2014) DOI 10.1007/s11051-014-2475-2
Articles 2013
Investigation of the rheological behavior of industrial tubular and autoclave LDPEs under SAOS, LAOS, transient shear, and elongational flows compared with predictions from the MSF theory M. Abbasi, N. Golshan Ebrahimi, M. Wilhelm; Journal of Rheology 57 1693-1714 (2013); DOI:10.1122/1.4824364
RAFT-based Polystyrene and Polyacrylate Melts under Thermal and Mechanical Stress O. Altintas, K. Riazi, R. Lee, C.Y. Lin, M. L. Coote, M. Wilhelm, C. Barner-Kowollik; Macromolecules 46 8079-8091 (2013); DOI: 10.1021/ma401749h
Effect of Polymer Structure and Incorporation of Nanoparticles on the Behavior of Syndiotactic Polypropylenes J. Bejarano, R. Benavente, E. Pérez, M. Wilhelm, R. Quijada, H. Palza; Macromol. Chem. Phys. 214 2567-2578 (2013); DOI: 10.1002/macp.201300392
Staudinger’s time in Karlsruhe and his later relations with Karlsruhe M. Wilhelm; Adv. Polym. Sci. 261 53 (2013)
A Combined NMR Relaxometry and Surface Instability Detection System for Polymer Melt Extrusion K.-F. Ratzsch, R. Kadar, I. F. C. Naue, M. Wilhelm; Macromol Mater Eng 298 1124-1132 (2013); DOI: 10.1002/mame.201300243
Seawater desalination via hydrogels: Practical realisation and first coarse grained simulations J. Höpfner, T. Richter, P. Košovan, C. Holm, M. Wilhelm; Prog. Coll. Polym. Sci. 140 247-263 (2013); DOI 10.1007/978-3-319-01683-2_19
Crosslinked Poly(ethylene oxide) as a Versatile Alignment Medium for the Measurement of Residual Anisotropic NMR Parameters C. Merle, G. Kummerlöwe, J.C. Freudenberger, F. Halbach, W. Stöwer, C.L v. Gostomski, J. Höpfner, M. Wilhelm, B. Luy; Angew. Chem. Int. Ed. 52 10309-10312 (2013); DOI 10.1002/anie.201301929
 
Combined methods in Rheology: Rheo-SAXS, Rheo-NMR and Rheo-Dielectric to gain unique correlations N. Dingenouts, T. Meins, K. Hyun, B. Struth, K. Ratzsch, C. Friedrich, G. Guthausen, M. Wilhelm; Proceedings of the Polymer Processing Society PPS29 July, Nueremberg, Germany(2013)
Rheological behavor and crystallization of PS-PLLA block copolymers   A. Malek, N. Dingenouts, T.F. Beskers, U. Fehrenbacher, L. Barner, M. Wilhelm; Eur. Polym. J. 49 2704-2720 (2013); DOI 10.1016/j.eurpolymj.2013.05.031
Synthesis and Linear and Nonlinear Melt Rheology of Well-Defined Comb Architectures of PS and PpMS with a Low and Controlled Degree of Long-Chain Branching M. Kempf, D. Ahirwal, M. Cziep, M. Wilhelm; Macromolecules 46, 4978-4994 (2013); DOI 10.1021/ma302033g
Validity of the modified molecular stress function theory to predict the rheological properties of polymer nanocomposites H.M. Hassanabadi, M. Abbasi, M. Wilhelm, D. Rodrigue; J. Rheol. 57, 881-899 (2013); doi: 10.1122/1.4798559
April-Science: Charakterisierung von hellen und dunklen Bierschäumen durch mechanische Obertonanlyse, FT-Rheologie K. Reinheimer, M. Wilhelm; Bunsenmagazin 15 52-55 (2013);
Effect of Short-Chain Branching on the Melt Behavior of Polypropylene Under Small-Amplitude Oscillatory Shear Conditions H. Palza , R. Quijada , M. Wilhelm; Macromol. Chem. Phys. 214 107-115 (2013); DOI 10.1002/macp.201200391
From self-assembly of electrospun nanofibers to 3D cm thick hierarchical foams D. Ahirwal, A. Hebraud, R. Kadar, M. Wilhelm, G. Schlatter; Soft Matter 9 3164-3172 (2013); DOI 10.1039/C2SM27543K

Das Entropierad : Maschine aus Konformationsänderungen

I.F.C. Naue, M. Wilhelm; Phys. in uns. Zeit 44 36-39 (2013); DOI 10.1002/piuz.201301318
Numerical Simulation results of the New Nonlinear Coefficient Q from FT-Rheology using a single mode Pom-Pom model K. Hyun, S.J. Park, M. Wilhelm; J. Rheol. 57 1-25 (2013; DOI 10.1122/1.4754444
Anomalous small-angle x-ray scattering from mesoporous noble metal catalysts K. Vogtt, G. Goerigk, M. Ballauff, R. Glaeser, N. Dingenouts; Colloid and Polymer Science 291 2163-2171 (2013; DOI 10.1007/s00396-013-2951-8
Articles 2012
Two dimensional Fourier Transform Rheological Study of Thermosensitivity Poly(N,N-diethylacrylamide) in aqueous solutions S. Strandman,  D.G. Lessard, D. van Dusschoten, M. Wilhelm, P.M. Wood-Adams, H.W. Spiess, X.X. Zhu; Polymer 53 4800-4805 (2012); DOI 10.1016/j.polymer.2012.08.028
Online Coupling of Size Exclusion Chromatography and Low Field NMR-Spectroscopy M. Cudaj, G. Guthausen, T. Hofe, M. Wilhelm; Macromol. Chem. Phys. 213 1933-1943 (2012); DOI 10.1002/macp.201200290
Multi-Block Polyurethanes via RAFT End-group Switching and their Characterization by Advanced Hyphenated Techniques C. Schmid, J. Falkenhagen, T.F. Beskers, L.-T. T. Nguyen, M. Wilhelm, F.D.Du Prez, C. Barner-Kowollik; Macromolecules 45 6353-6362 (2012); DOI 10.1021/ma301117k
Online Coupling of Size Exclusion Chromatography and FT-IR-Spektroscopy T. F. Beskers, T. Hofe, M. Wilhelm; Macromol. Rapid Commun. 33 1747-1752 (2012);DOI 10.1002/marc.201290071
Optimizing the sensitivity of FT-Rheology to quantify and differentiate for the first time the nonlinear mechanical response of dispersed beer foams of light and dark beer

K. Reinheimer, J. Kübel, M. Wilhelm;  Z. Phys. Chem. 226 p547-567 (2012); DOI 10.1524/zpch.2012.0247

In-situ Rheo-Dielectric, ex-situ 2D-SAXS and FT-Rheology investigations of the shear induced alignment of Poly(styrene-b-1,4-isoprene) diblock copolymer melts T. Meins, N. Dingenouts, J. Kübel, M. Wilhelm;  Macromolecules 45 7206-7219 (2012); DOI 10.1021/ma300124b
Polystyrene solutions: characterization of molecular motional modes by spectrally resolved low and high field NMR relaxation M. Cudaj, J. Cudaj, T. Hofe, B. Luy, M. Wilhelm, G. Guthausen; Macromol. Chem. Phys. 213 1833-1840 (2012; DOI 10.1007/s00723-014-0522-x
Development of a low field Rheo-NMR System K. Ratzsch, A. Hoffmann, C. Friedrich, M. Wilhelm; 25 Intern. Symp. on Polymer Analysis and Characterization (ISPAC); 32 (2012) ISBN 978-90-365-3352-2
Online coupling of size exclusion chromatography and IR-Spectroscopy to correlate molecular weight with chemical composition T. Beskers, T. Hofe, M. Wilhelm; 25 Intern. Symp. on Polymer Analysis and Characterization (ISPAC); 12 (2012) ISBN 978-90-365-3352-2
Combined methods in Rheology: Rheo-SAXS, Rheo-NMR, and Rheo-Dielectric to bridge length and time scales M. Wilhelm; Proceedings 6th Intern. Symp. on Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 82 (2012) ISBN 978-3-905609-49-3
Fourier Transform Rheology as a noninvasive characterization technique for emulsions K. Reinheimer, M. Grosso, J. Kübel, F. Hetzel, M. Wilhelm; Proceedings 6th Internat. Symp. on Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 45 (2012) ISBN 978-3-905609-49-3
Fourier Transform Rheology as a noninvasive morphological characterization technique for the emulsion volume average radius and its distribution K. Reinheimer, M. Grosso, F. Hetzel, J. Kübel, M. Wilhelm; J. Colloid Interface Sci. 380 201-212 (2012); DOI 10.1016/j.jcis.2012.03.079
Electrical, Thermal and Mechanical Characterization of Polypropylene/Carbon Nanotube/Clay Hybrid Composite Materials H. Palza, B. Reznick, M. Wilhelm, O. Arias, A. Vargas; Macromol. Mater. Eng. 297 474-480 (2012); DOI 10.1002/mame.201100249
New insight to the mechanism of shear-induced macroscopic alignment of diblock copolymer melts by a unique and newly developed Rheo-SAXS combination T. Meins, K. Hyun, N. Dingenouts, B. Struth, M. Wilhelm; Macromolecules 45 455-473 (2012); DOI 10.1021/ma201492n
Experiments on elastic cloaking in thin plates N. Stenger, M. Wilhelm, M. Wegener; Phys. Rev. Letters 108 014301 (2012); DOI 10.1103/PhysRevLett.108.014301
Acyclic Triene Metathesis Polymerization of Plukenetia conophora oil: branched polymers by direct polymerization of renewable resources C.O. Akintayo, H. Mutlu, M. Kempf, M. Wilhelm, M.A.R. Meier; Macromol. Chem. Phys. 213 87-96 (2012); DOI 10.1002/macp.201100539
Small angle X-ray scattering study of formation of colloidal silica Stoeber multiplets V. Goertz, A. Gutsche, N. Dingenouts, H. Nirschl, J Phys Chem C 116 26938-26946 (2012); DOI 10.1021/jp3111875
ZnO nanocontainers: structural study and controlled release P. Leidinger, N. Dingenouts, R. Popescu, D. Gerthsen, C. Feldmann; J. Mater. Chem 22 14551-14558 (2012); DOI10.1039/C2JM31609A
Articles 2011
Neuartige Meerwasserentsalzung mit Hilfe von polymeren Hydrogelen J. Höpfner, M. Wilhelm; 7. Thüringer Grenz- und Oberflächentage; Hrsg.: Innovent e.V.; Jena 2011; S. 87 – 91, ISBN: 978-3-00-035347-5
Nested dipolar Halbach array for the determination of magnetorheological properties at variable magnetic field V.C. Barroso, H. Raich, P. Blümler, H.W. Spiess, M. Wilhelm; Rheol. Acta 50 441-459 (2011); DOI 10.1007/s00397-011-0578-6
Linear and non-linear rheology of industrial linear polyethylenes I. Vittorias, D. Lilge, V.C. Barroso, M. Wilhelm; Rheol Acta 50 691-700 (2011); DOI 10.1007/s00397-011-0561-2
Morphological changes of carbon nanotubes in polyethylene matrices under oscillatory tests as determined by dielectrical measurements H. Palza, M. Kappes, F. Heinrich, M. Wilhelm;  Composites Science and Technology 71 1361-1366 (2011); DOI 10.1016/j.compscitech.2011.05.010
Fourier Transform Rheology as a universal non-linear mechanical characterization of droplet size and interfacial tension of dilute monodisperse emulsions K. Reinheimer, M. Grosso, M. Wilhelm; J. Colloid Interface Sci. 360 818-825 (2011) DOI 10.1016/j.jcis.2011.05.002
A Review on Nonlinear Oscillatory Shear tests: Analysis and Application of Large Amplitude Oscillatory shear (LAOS) K. Hyun, C.O. Klein, M. Wilhelm, K.S. Cho, J.G. Nam, K.H. Ahn, S.J. Lee, R.H. Ewoldt, G.H. McKinley; Prog. Polym. Sci. 36 1697-1753 (2011); DOI 10.1016/j.progpolymsci.2011.02.002
Sperulite Growth Rate in Polypropylene/Silica Nanoparticle Composites: Effefct of Particle Morphology and Compatibilizer H. Palza, J. Vera, M. Wilhelm, P. Zapata;  Macromol. Mater. Eng. 296 744-751 (2011); DOI 10.1002/mame.201000405
A new non-linear Parameter for polymer melts, using FT-Rheology K. Hyun, M. Kempf, D. Ahirwal, V.H. Rolón-Garrido, M.H. Wagner, M. Wilhelm;  Annual Transactions the Nordic Rheology Society, 19 247 (2011), ISBN 978-952-15-2589-6
Combined methods in Rheology: Rheo-SAXS, Rheo-NMR and Rheo-Dielectric to bridge length and time scales T. Meins, K. Hyun, K. Ratzsch, C. Friedrich, B. Struth, M. Wilhelm;  Annual Transactions the Nordic Rheology Society, 19 201 (2011), ISBN 978-952-15-2589-6
Linear and non-linear viscoelastic rheology of hybrid nanostructured materials from block copolymers with gold nanoparticles C. Mendoza, N. Gindy, A. Fahmi, M. Wilhelm; Rheol. Acta 50 257-275 (2011); DOI 10.1007/s00397-011-0540-7
Observation of new states of liquid crystal 8CB under non-linear shear conditions as observed via a novel and unique Rheo/Small Angle X-ray scattering combination B. Struth, K. Hyun, E. Kats, T. Meins, M. Walther, M. Wilhelm, G. Grübel; Langmuir 27 2880-2887 (2011); DOI 10.1021/la103786w
Analysis of Medium Amplitude Oscillatory Shear data of entangled linear and comb polymer model systems M. H. Wagner, V. H. Rolón-Garrido, K. Hyun, M. Wilhelm; J. Rheol. 55 495-516 (2011); DOI 10.1122/1.3553031
SEC-MR-NMR: Online Coupling of Size Exclusion Chromatography and Medium Resolution NMR Spectroscopy M. Cudaj, G. Guthausen, A. Kamlowski, D. Maier, T. Hofe, M. Wilhelm; Macromol. Rapid Commun. 32 665-670 (2011); DOI 10.1002/marc.201000760
Medium Resolution NMR at 20 MHz: Possibilities and Challenges M. Cudaj, T. Hofe, M. Wilhelm, M.A. Vargas, G. Guthausen; Magnetic Resonance in Food Science 83 (2011); DOI 10.1039/9781849732994-00083
New methods for the rheological characterisation of materials M. Wilhelm; Chem. Eng. Process. 50 486 (2011); DOI 10.1016/j.cep.2010.06.006
Molecular dynamics of ionic liquids as Probed by rheology N. Pogodina, M. Nowak, J. Läuger, C.O. Klein, M. Wilhelm, C. Friedrich; J. Rheol. 55 241-256 (2011); DOI 10.1122/1.3528651
Formation of Triblock Copolymers via a Tandem Enhanced Spin Capturing—Nitroxide-Mediated Polymerization Reaction Sequence T. Junkers, L. Zang, E.H.H. Wong, N. Dingenouts, C. Barner-Kowollik; Journal of Polymer Science A49 4841–4850 (2011); DOI 10.1002/pola.24970
An Access Route to Polyferrocenes via Modular Conjugation C. Lang, D. Voll, AJ. Inglis, N. Dingenouts, A. Goldmann, L. Barner, C. Barner-Kowollik; Macromolecular Chemistry and Physics, 212 831-839 (2011); DOI 10.1002/macp.201100010
Articles 2010
New developments for the mechanical characterization of materials N. Dingenouts, M. Wilhelm; AnwenderSeminar TA-Instruments, Würzburger Tage 2010, p 123, ISBN 978-3-940184-08-5 (2010)
New developments for the mechanical characterization of materials N. Dingenouts, M. Wilhelm; Korea-Australia Rheology Journal 22 317-330 (2010)
Nonliner response of dense colloidal suspensions under oscillatory shear: Mode-coupling theory and FT-rheology experiments J.M. Brader, M. Siebenbürger, M. Ballauff, K. Reinheimer, M. Wilhelm, S.J. Frey, F. Weyßer, M. Fuchs; Phys. Rev. E 82 061401/1-20 (2010); DOI 10.1103/PhysRevE.82.061401
A spectrometer for the spectrally resolved low-field NMR M. Cudaj, G. Guthausen, A. Kamlowski, D. Maier, T. Hofe, M. Wilhelm; Nachrichten aus der Chemie 58 1155-1157 (2010); DOI 10.1002/nadc.201075952
Determination of the non-linear parameter (mobility factor) of the Giesekus constitutive model using LAOS procedure A. Calin, M. Wilhelm, C. Balan; J. Non-Newtonian Fluid Mech  165 1564-1577 (2010); DOI 10.1016/j.jnnfm.2010.08.008
Anionic Synthesis and Rheological Characterization of Poly(p-methylstyrene) Model Comb Architectures with a Defined and Very Low Degree of Long Chain Branching (LCB) M. Kempf, V.C. Barroso, M. Wilhelm; Macromol. Rap. Comm. 31 2140-2145 (2010); DOI 10.1002/marc.201000412
Characterization of melt flow instabilities in polyethylene/carbon nanotube composites H. Palza, B. Reznik, M. Kappes, F. Hennrich, I.F.C. Naue, M. Wilhelm; Polymer 51 3753-3761 (2010); DOI 10.1016/j.polymer.2010.06.016
On-line Detection of Polymer Melt Flow Instabilities in a Capillary Rheometer H. Palza, I.F.C. Naue, S. Filipe, A. Becker, J. Sunder, A. Göttfert, M. Wilhelm; Kautsch. Gummi Kunstst. 63 456-461 (2010)
Silane-Functionalized Flame Retardent Aluminum Trihydroxide in Flexible Polyurethane Foam A. König, A. Malek, U. Fehrenbacher, G. Brunklaus, M. Wilhelm, T. Hirth; Journal of Cellular Plastics 46 395-413 (2010); DOI 10.1177/0021955X10367703
A Novel Approach for the Desalination of Seawater by Means of Reusable Poly(acrylic acid) Hydrogels and Mechanical Force J. Hoepfner, C. Klein, M. Wilhelm; Macromol. Rap. Comm. 31 1337-1342 (2010); DOI 10.1002/marc.201000058
Non-linear rheology of entangled linear and branched polymer melts under large amplitude oscillatory shear K. Hyun, M. Wilhelm; Kautsch. Gummi Kunstst. 63 123-129 (2010)
Correlation between polyethylene topology and melt flow instabilities by determining in-situ pressure fluctuations and applying advanced data analysis H. Palza, S. Filipe, I.F.C. Naue, M. Wilhelm; Polymer 51 522-534 (2010); DOI 10.1016/j.polymer.2009.11.050
Self-Organization of Coil-Ring-Coil Structures into Tubular Supramolecular Polymer Brushes: Synthesis, Morphology, and Growth M. Fritzsche, S. Jester, S. Hoeger, C. Klaus, N. Dingenouts, P. Linder, M. Drechsler, S. Rosenfeldt; Macromolecules 43 8379-8388 (2010); DOI 10.1021/ma1016242
Single chain self-assembly: preparation of alpha,omega-donor-acceptor chains via living radical polymerization and orthogonal conjugation O. Altintas, P. Gerstel, N. Dingenouts and C. Barner-Kowollik; Chem. Comm. 46 6291-6293 (2010); DOI 10.1039/c0cc00702a
Online Low-Field (1)H-NMR Spectroscopy: Monitoring of Emulsion Polymerization of Butyl Acrylate M.A. Vargas, M. Cudaj, K. Hailu, K. Sachsenheimer, G. Guthausen; Macromolecules 43, 5561-5568 (2010); DOI 10.1021/ma1006599
Articles 2009
Synthese und Charakterisierung von Polyestern und Polyamiden auf der Basis von Furan-2,5-dicarbonsäure O. Grosshardt, B. Tübke, K. Kowollik, U. Fehrenbacher, N. Dingenouts, M. Wilhelm; Chemie Ingenieur Technik 81 1829 (2009); DOI 10.1002/cite.200900090
Structural and mechanical characterization of k/i-hybrid carrageen gels in potassium salt using Fourier Transform rheology L. Hilliou, M. Wilhelm, M.P. Goncalves; Food Hydrocolloids 23 2322-2330 (2009; DOI 10.1016/j.foodhyd.2009.06.008
In-situ Pressure Fluctuations of Polymer Melt Instabilities in a Viscoelastic Poisseule Flow: Experiemntal Evidence about their Origin and Dynamics H. Palza, I.F.C. Naue, M. Wilhelm; Macromol. Rapid Commun. 30 1799-1804 (2009); DOI 10.1002/marc.200900296
Addition of the force measurment capability to a commercial available extensional rheometer (CaBER) C.O. Klein, I.F.C. Naue, J. Nijmann, H. Buggisch, M. Wilhelm; Soft Materials 7 242-257 (2009); DOI 10.1080/15394450903344603
Interplay between Microstructure and Mechanical Properties in Carrageenan Gels in NaCl Salt and in Gelatin Gels L. Hilliou, M.P. Goncalves, M. Wilhelm; Proceedings of the 5^th International Symposium on Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 306 (2009)
Mechanical Analysis of Model Emulsions and Estimation of the Particle Size both based on FT-Rheology C.O Klein, K. Reinheimer, M. Wilhelm; Proceedings of the 5^th International Symposium on Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 130 (2009)
Polymer motion as detected via dielectric spectra of 1,4-cis-polyisoprene under large amplitude oscillatory shear (LAOS)

K. Hyun, S. Höfl, S. Kahle, M. Wilhelm; 
J. Non-Newtonian Fluid Mech 160 93-103 (2009); DOI 10.1016/j.jnnfm.2009.03.002

Detection and Quantification of Branching in Polyacrylates by Size-Exclusion Chromatography (SEC) and melt-state NMR

P. Castignolles, R. Graf, M. Parkinson, M. Wilhelm, M. Gaborieau; Polymer 50 2373 (2009); DOI 10.1016/j.polymer.2009.03.021

Mechanische Eigenschaften mit Obertonanalyse: FT-Rheologie

M. Wilhelm;
Nachrichten aus der Chemie 57 422-425 (2009); DOI 10.1002/nadc.200963083

Double dipolar Halbach array for rheological measurements on magnetic fluids at variable magnetic flux density B V.C. Barroso, H. Raich, P. Blümler, M. Wilhelm; Journal of Physics: Conference Series 149 012102 (2009); DOI 10.1088/1742-6596/149/1/012102
Evaluation of melt flow instabilities of high-density Polyethylenes via an optimised method for detection and analysis of the pressure fluctuations in capillary rheometry S. Filipe, A. Becker, V.C. Barroso, M. Wilhelm; Applied Rheology 19 23345 (2009); DOI 10.3933/ApplRheol-19-23345
Establishing a New Nonlinear Coefficient Q from FT-Rheology, first investigations on entangled linear and branched Polymer melts K. Hyun, M. Wilhelm;
Macromolecules 42 411-422 (2009); DOI 10.1021/ma8017266
Comparison of Nanometric Particle Size Distributions determined by SAXS, TEM and Analytical Ultracentrifuge V. Goertz, N. Dingenouts and H. Nirschl; Particle & Particle Systems Characterization 26 17-24 (2009); DOI 10.1002/ppsc.200800002
Temperature induced switching between aggregated and non-aggregated states in coil-ring-coil block copolymers N. Dingenouts, S. Klyatskaya and S. Höger; Macromolecules 42 5900-5902 (2009); DOI 10.1021/ma901022w
Articles 2008
Experimental Results on Fourier Transform Rheology of PBLG/m-cresol and HPC/Water Liquid Crystalline Solutions M.T. Cidada, S. Filipe, V.C. Barroso, M. Wilhelm; Mol. Cryst. Liq. Cryst. 495 247 (2008); DOI 10.1080/15421400802430208
Extending the Capabilities of the CaBER with Highly Sensitive Force Measurments C. Klein, I. Naue, M. Wilhelm, R. Brummer, J. Nijman; Proceedings of the XV-th International Congress on Rheology 1208 (2008)
Establishing a New Nonlinear Q Parameter from FT-Rheology First Investigations on Monodisperse Polymer Melts K. Hyun, M. Wilhelm; Proceedings of the XV-th International Congress on Rheology 369 (2008)
A new Approach to Determine the Nonlinear Parameter of the Gisekus Constitutive Model A. Calin, C. Balan, M. Wilhelm; Proceedings of the XV-th International Congress on Rheology 1372 (2008)
In-situ Rheo-SAXS Study of Shear Induced Alignment of Liquid Crystal (8CB) in the Smectic Phase under LAOS K. Hyun, B. Struth, T. Meins, M. Wilhelm; Proceedings of the XV-th International Congress on Rheology 1423-1425 (2008)
Measurement of the Rheological of Magnetorheological Fluids Using a Double Concentric Halbach Cylinder Array V.C. Barroso, H. Raich, P. Blümler, M. Wilhelm; Proceedings of the XV-th International Congress on Rheology 1144 (2008)
Combination of NMR relaxometry and mechanical testing during vulcanisation S. Kahle, M. Hehn, H.P. Raich, W. Nussbaum, P. Blümler, M. Wilhelm; Kautsch. Gummi Kunstst. 61 92-94 (2008)
Experimental correlation between mechanical non-linearities in LAOS flow and capillary flow instabilities for linear and branched commercial polyethylenes S. Filipe, I. Vittorias, M. Wilhelm; Macromol. Mat. Eng. 293 57 (2008); DOI 10.1002/mame.200700194
Articles 2007
Combination of NMR Relaxometry and Mechanical Testing during Vulcanisation S. Kahle, M. Hehn, H.P. Raich, W. Nussbaum, P. Blümler, M. Wilhelm; 11-th International Semiar on Elastomers, 91 (2007)
3D Microstructured surface obtained by soft-lithography using fast-cross elastomeric precursors and 2D master A. del Campo, I. Alverez, S. Filipe, M. Wilhelm; Adv. Funct. Mater. 17 3590 (2007); DOI 10.1002/adfm.200700132
Application of FT-Rheology towards industrial linear and branched polyethylene blends I. Vittorias, M. Wilhelm; Macromol. Mat. Eng. 292 935 (2007); DOI 10.1002/mame.200700120
Effect of branch length on NMR relaxation properties in molten polyethylene-co-a-olefin model systems M. Parkinson, K. Klimke, H.W. Spiess, M. Wilhelm; Macomol. Chem. Phys. 208 2128-2133 (2007); DOI 10.1002/macp.200700209
Kinetics of shear microphase orientation and reorientation in lamellar diblock and triblock copolymer melts as detected via FT-Rheology and 2D-SAXS C. Oelschlager, J.S. Gutmann, M. Wolkenauer, H.W. Spiess, K. Knoll, M. Wilhelm; Macromol. Chem. Phys. 208 1719-1729 (2007); DOI 10.1002/macp.200700150
Optimized rheo-optical measurements using Fast Fourier Transform and oversampling C. Klein, P. Venema, L. Sagis, D. van Dusschoten, M. Wilhelm, H.W. Spiess, E. van der Linden, S. Rogers, A.M. Donald; Applied Rheology 17 45210 (2007); DOI 10.3933/ApplRheol-17-45210
Separation of the non-linear oscillatory shear response, into a superposition of linear, strain hardening, strain softening and wall slip response

C. Klein, H.W. Spiess, A. Calin, C. Balan, M. Wilhelm; Macromolecules 40 4250-4259 (2007); DOI 10.1021/ma062441u

Detection of the long-chain branching in polyolefines via Fourier-Transform Rheology and finite element simulations

I. Vittorias, M. Wilhelm;
Kautsch. Gummi Kunstst. 60 112 (2007)

Detection and quantification of industrial polyethylene branching topologies via Fourier-Transform Rheology and simulation using the Pom-Pom model I. Vittorias, M. Parkinson, K. Klimke, B. Debbaut, M. Wilhelm; Rheol. Acta 46 321-340 (2007); DOI 10.1007/s00397-006-0111-5
Characterizing dispersion and fragmentation of fractal, pyrogenic silica nanoagglomerates by small angle X-ray scattering R. Wengeler, F. Wolf, N. Dingenouts and H. Nirschl; Langmuir 23 4148-4154 (2007), DOI 10.1021/la063073q
Formation of Triblock Copolymers via a Tandem Enhanced Spin Capturing—Nitroxide-Mediated Polymerization Reaction Sequence T. Junkers, L. Zang, E.H.H. Wong, N. Dingenouts, C. Barner-Kowollik; Journal of Polymer Science A49 4841–4850 (2011); DOI 10.1002/pola.24970
Articles 2006
Introduction to Rheology of Polymers

M. Wilhelm; E-Seminar Darmstadt-Berkeley (2006) invited internet contribution by Prof. P. Hagedorn

Effect of large amplitude oscillatory shear (LAOS) on the dielectric response of 1,4-cis-polyisoprene S. Höfl, F. Kremer, H.W. Spiess, M. Wilhelm, S. Kahle; Polymer 47 7282-7288 (2006)
Solid state NMR investigations on the role of organic admixtures on the hydration of cement pastes

J. Rottstegge, M. Wilhelm, H.W. Spiess; Cement and Concrete Research 28 417 (2006)

Small-angle X-ray scattering and linear melt rheology of Poly(tert-butylacrylate-g-styrene) graft copolymers J.L. de la Fuente, M. Fernández-Garcia, M.L. Cerrada, E.L. Madruga, H.W. Spiess, M. Wilhelm; Polymer 47 1487 (2006)
Separation of the linear response, as detected via FT-Rheology, into physica phenomena C. Klein, H.W. Spiess, M. Wilhelm; Proc. 4th Int. Symp. Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 735 (2006)
Kinetics of shear microphase orientation in lamellar triblock copolymer melts as detected via FT-Rheology and 2D-SAXS C. Oelschlaeger, J. Gutmann, M. Wolkenhauer, H.W. Spiess, K. Knoll, M. Wilhelm; Proc. 4th Int. Symp. Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 729 (2006)
Characterization of the linear and nonlinear rheological response of pea protein/kappa-Carrageenan solution including the dynamics of gel formatin R. Musampa, M. Wilhelm, J. Maia; Proc. 4th Int. Symp. Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 673 (2006)
Shear microphase orientation and reorientatin in lamellar diblock and triblock copolymer melts as detected via FT-Rheology and 2D-SAXS C. Oelschlaeger, J. Gutmann, M. Wolkenhauer, H.W. Spiess, K. Knoll, M. Wilhelm; Proc. 4th Int. Symp. Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 487 (2006)
Influence of comonomer type and content on lang.chain branching of ethylene-/a-olefin copolymers F.J. Stadler, C. Piel, K. Klimke, J. Kaschta, M. Parkinson, W. Kaminsky, M. Wilhelm, H. Münstedt; Macromolecules 39 1472 (2006)
Optimisation and Application of Polyolefin Branch Quantification by Melt-State 13C NMR Spectroscopy K. Klimke, M. Parkinson, C. Piel, W. Kaminsky, H.W. Spiess; M. Wilhelm; Macromol. Chem. Phys. 207 382-395 (2006)
Large Amplitude Oscillatory shear behaviour of PEO-PPO-PEO triblock copolymer solutions K. Hyun, J.G. Nam, M. Wilhelm, K.H. Ahn, S.J. Lee; Rheol. Acta 45 239 (2006)
Evolution of morphological and rheological properties along the extruder length for compatibilized blends of a commercial liquid crystalline polymer and polypropylene S. Filipe, M.T. Cidada, M. Wilhelm, J.M. Maia;
J. Appl. Polym. Sci. 99 347 (2006)
Articles 2005
FT-Rheologie an Hochleistungsmaterialien M. Wilhelm; Anwenderseminar TA-Instruments, S.39, Würzburg (2005)
Solid State NMR and LVSEM studies on the hardening of latex modified tile mortar systems J. Rottstegge, M. Arnold, L. Herschke, G. Glasser, M. Wilhelm, H.W. Spiess, W.D. Hergeth; Cement and Concrete Research 35 2233 (2005)
Photorheology of Fast UV Curing Multifunctional Acrylates L.E. Schmidt, Y. Leterrier, J.-M. Vesin, M. Wilhelm, J.-A.E. Manson; Macromol. Mat. Eng. 290 1115 (2005)
Thermal, Morphological and Rheological Characterization of Poly(acrylic acid-g-styrene) Amphiphilic Graft Copolymers J.L. de la Fuente, M. Wilhelm, H.W. Spiess, E.L. Madruga, M. Fernández-Garcia, M.L. Cerrada; Polymer 46 4544 (2005)
FT-Rheology: a very sensitive experimental technique to characterize the non-linear regime in materials M. Wilhelm; Kautsch. Gummi Kunstst. 58 256 (2005)
Articles 2004
Evolution of morphological and rheological properties along the extruder length for blends of a commercial liquid crystalline polymer and polypropylene S. Filipe, M.T. Cidade, M. Wilhelm, J.M. Maia;
Progress in Rheology of Biological and Synthetic Polymer Systems; ISBN 972-99301-0-4, 419 (2004)
FT-Rheology: a very sensitive experimental technique to characterize the non-linear regime in materials M. Wilhelm;
6-th Fall rubber Colloquium 31 (2004)
Distinguish linear from star-branched polystyrene solutions with Fourier-Transform Rheology T. Neidhöfer, S. Stella, N. Hadjichristidis, M. Wilhelm; Macromol. Rap. Commun. 25 1921 (2004)
FT-Rheology, a very sensitive experimental technique to characterize the non-linear regime in materials

M. Wilhelm; Prog. in Rheology of Bio. & Syn. Polymer Systems; ISBN 972-99301-0-4, 3 (2004)

Fourier-Transform Rheology to distinguish polymer solutions with different Topologies T. Neidhöfer, M. Wilhelm; Rheofuture (2004) http://www.rheofuture.de/
Increasing the Torque Transducer Sensitivity of an RPA 2000 by a factor 5 – 10 using advanced data acquisition L. Hilliou, D. van Dusschoten, M. Wilhelm, H. Burhin, E.R. Rodger; Rubber Chemistry and Technology 77 192-200 (2004)
Evolution of morphological and rheological properties along the extruder length for blends of a commercial liquid crystalline polymer and polypropylene S. Filipe, M.T. Cidade, M. Wilhelm, J.M. Maia;
Polymer 45 2367 (2004)
Observation of chain branching in polyethylene in the solid-state and melt via 13C-NMR spectroscopy and melt NMR relaxation time measurements M. Pollard, K. Klimke, R. Graf, H.W. Spiess, M. Wilhelm, O. Sperber, C. Piel, W. Kaminsky; Macromolecules 37 813-825 (2004)
Articles 2003
Topology in polyolefines as seen by solid-state NMR and FT-Rheology M. Wilhelm, M.A.  Pollard, R. Graf, K. Klimke, H.W. Spiess, O. Sperber, C. Piel, W. Kamanisky; Abs. Pap. ACS 226: U388-U388-Poly Part 2 Sept. 2003
Expanding the detection limit for side chain branches in polyethylene: 13C NMR spin lattice relaxation and NOE buildup directly in the melt M. Pollard, M. Wilhelm, H.W. Spiess, O. Sperber, C. Piel, W. Kamanisky; Abs. Pap. ACS 226: U632-U632-Poly Part 2 March 2003
Structural Studies of Nanophase Separated Poly(2-hydroxyethylmethacrylate)-l-Polyisobutylene Amphiphilic Co-networks by Solid-State-NMR and Small Angle X-Ray Scattering A. Domján, G. Erdodi, M. Wilhelm, M. Neidhöfer, K. Landfester, B. Iván, H.W. Spiess; Macromolecules 36 9107 (2003)
Domain Size Determination of Poly(phthalamide)/Poly-(dimethylsiloxanes) Block Copolymer by 1H Solid-State Spin Diffusion NMR Spectroscopy A. Kretschmer, R.A. Drake, S.J. Jones, M. Neidhoefer, M. Wilhelm, H.W. Spiess; Organosilicon Chemistry V, Editors: Norbert Auner, Johann Weis; Wiley-VCH: Weinheim, Germany, 2003, 339-343
The influence of sodium ethene sulfonate comonomer on the film formation process of poly(vinyl acetate) dispersion J. Rottstegge, P. Kindervater, M. Wilhelm, K. Landfester, C. Heldmann J.P. Fischer, H.W. Spiess; Colloid & Polymer Science 281 1111 (2003)
Fourier-Transform rheology experiments and finite-element simulations on linear polystyrene solutions T. Neidhöfer, M. Wilhelm, B. Debbaut;
J. Rheol. 46 1351 (2003)
Non-linear response under large amplitude oscillatory shear flow K. Hyun, J.G. Nam, M. Wilhelm, K.H. Ahn, S.J. Lee; Korea-Aust. Rheol. J. 15 97( 2003)
Expanding the detection limit for side-chain branches in polyethylene: 13C NMR Spin-lattice relaxation and NOE buildup directly in the melt M. Pollard, H.W. Spiess, M. Wilhelm, O. Sperber, C. Piel, W. Kaminsky; ACS preprint 225, Poly, March 23, (2003)
Kinetics of Isothermal Crystallization in isotactic Polypropylene Monitored with Rheology and FT-Rheology T. Dötsch, M. Pollard, M. Wilhelm;
J. Phys.: Cond. Mat. 15 S923-S931 (2003)
Investigations on the film formation process of latex dispersions by solid-state NMR J. Rottstegge, B. Traub, M. Wilhelm, K. Landfester, C. Heldmann, HW. Spiess; Macromol. Chem. Phys. 204 787 (2003)
Effect of Interfaces on the Crystallization Behavior of PDMS T. Dollase, Y. Yagen, M. Wilhelm, H.W. Spiess, R. Yerushalmi-Rozen, M. Gottlieb; Interface Science 11 199-209 (2003)
Characterisation of model dispersions by Fourier-Transform Rheology C. Klein, L. Hilliou, M. Wilhelm; Proc. 3th Int. Symp. Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 449 (2003)
Microphase Reorientation in a Block Copolymer Melt as detected by FT-Rheology and 2D-SAXS M. Langela, M. Wilhelm; Proc. 3th Int. Symp. Food Rheology and Structure (ISFRS); Kerschensteiner Verlag 229 (2003)
Articles 2002
FT-Rheology and Finite-Element Simulations on Polystyrene Solutions and Melts of Various Topologies T. Neidhöfer, M. Wilhelm, B. Debbaut, N. Hadjichristidis; Proc. 6-th European Congress on Rheology 463 (2002)
Reorientation in a Block Copolymer Melt as Detected by a Combination of FT-Rheology and 2D-SAXS

M. Langela, M. Wilhelm; Proc. 6-th European Congress on Rheology 619 (2002)

Quantification of Composition and Domain Size of Industrial Poly(phthalamide)/Poly(dimethylsiloxane) Block Copolymers using Different 1H Solid-State NMR Methods A. Kretschmer, R. Drake, M. Neidhöfer, M. Wilhelm; Solid State Nucl. Magn. Reson. 22 204 (2002)
Trend Report in Macromolecular Chemistry S. Mayer, R. Zentel, M. Wilhelm, A. Greiner, D. Ulbrich, M. Vollmer; Macromol. Chem. Phys. 203 1743 (2002)
Microphase reorientation in block copolymer melts as detected via FT-Rheology and 2D-SAXS M. Langela, M. Wilhelm, U. Wiesner, H.W. Spiess; Macromolecules 35 3198-3204 (2002)
Trendberichte Makromolekulare Chemie 2001 S. Mayer, R. Zentel, M. Wilhelm, A. Greiner, D. Ulbrich, M. Vollmer; Nachrichten aus der Chemie 50 346 (2002), sowie 50 442 (2002)
Fourier-Transform Rheology

M. Wilhelm; Feature Artikel; Macromol. Mater. Eng. 287 83-105 (2002)

NMR studies of the structure and dynamics of polymer gels based on N-isopropylacrylamide (NiPAAm) and methacrylic acid (MAA)

E. Díez-Peña, I. Quijada-Garrido, J.M. Barrales-Rienda, M. Wilhelm, H.W. Spiess; Macromol. Chem. Phys. 203 491 (2002)

Articles 2001
Two-Dimensional Fourier-Transform Rheology D. van Dusschoten, M. Wilhelm, H.W. Spiess; J. Rheol. 45 1319 (2001)
Characterization of Polymer Dispersions by Fourier-Transform Rheology S. Kallus, N. Willenbacher, S. Kirsch, D. Distler, T. Neidhöfer, M. Wilhelm, H.W. Spiess; Rheol. Acta 40 552 (2001)
Blends of AB/BC Diblock Copolymers with a Large Interaction Parameter c H. Frielinghaus, N. Hermesdorf, R. Siegel, K. Almdal, K. Mortensen, I.W. Hamley, L. Messe, L. Corvazier, A.J. Ryan, D. van Dusschoten, M. Wilhelm, G. Floudas, G. Fytas; Macromolecules 34 4907 (2001)
Fourier-Transform Rheology on linear polystyrene melts T. Neidhöfer, M. Wilhelm, H.W. Spiess; Applied Rheology 11 126 (2001)
Increased Torque Transducer Sensitivity via Oversampling D. van Dusschoten, M. Wilhelm; Rheol. Acta 40 395-399 (2001)
Quantitative Characterisation of the Inner Structure of Core-Shell Latex Particles by 1H Solid-State NMR M. Valtier, X. Druion, M. Wilhelm, H.W. Spiess; Macromol. Chem. Phys. 202 1262 (2001)
Length Scale of Dynamic Heterogeneity in Glycerol near Tg S.A. Reinsberg, X.H. Qiu, M. Wilhelm, H.W. Spiess, M.D. Ediger; J. Chem. Phys. 114 7299 (2001)
Non-linear Rheology of a Face-centered Cubic Phase in a Diblock Copolymer Gel C. Daniel, I.W. Hamley, M. Wilhelm, W. Mingvanish; Rheol. Acta 40 39 (2001)
Articles 2000
Biolubrication: The shear of absorbed polyelectrolytes and of polymer brushes J. Klein, X.Y. Zhang, M. Wilhelm; Abs. Pap. ACS 219: 62-PMSE Part 2 March 26 2000 
Dynamics in the crystalline polymorphic forms I, II and form III of isotactic poly-1-butene D. Maring, M. Wilhelm, H.W. Spiess, B. Meurer, G. Weill; J. Poly. Sci. Part B: Polymer Physics 38 2611 (2000)
FT-Rheology to Quantify the Alignment kinetics in Blockcopolymers P. Reinheimer, M. Wilhelm, M. Langela, H. Leuninger, U. Wiesner, D. van Dusschoten; Proc. of the XIII-th International Congress on Rheology 1 287 (2000)
The Crossover between linear and non-linear mechanical behaviour in polymer solutions as detected by Fourier-Transform Rheology M. Wilhelm, P. Reinheimer, M. Ortseifer, T. Neidhöfer, H.W. Spiess; Rheol. Acta 39 241 (2000)
Modification of Surface Interactions and Friction by adsorbed dendrimers: 1. Low Surface Energy fifth-Generation Amino-Acid-Modified Poly(propyleneimine) Dendrimers X. Zhang, M. Wilhelm, J. Klein, M. Pfaadt, E.W. Meijer; Langmuir 16 3884 (2000)
Different Types of Water in the Film Formation Process of Latex Dispersions as Detected by Solid State NMR J. Rottstegge, K. Landfester, M. Wilhelm, H.W. Spiess, C. Heldmann; Colloid & Polymer Science 278 236 (2000)
LAOS Experiments in the Time Dependant, Non-linear regime Analyzed via Higher Harmonic Generation M. Wilhelm, T. Neidhöfer, D. van Dusschoten; Proc 2nd Int. Symp. Food Rheology and Structure; Kerschensteiner Verlag 113 (2000)
Articles 1999
Determination of the Provenance of two Archaeological amber beads from Romania by FTIR- and Solid-State-Carbon-13 NMR Spectroscopy

A. Bannerjee, V. Ghiurca, B. Langer, M. Wilhelm;  Archäologisches Korrespondenzblatt 29 593 (1999)

Quantitative Determination of Dynamic Heterogeneities in Core-Shell Latices by 1H-Solid State NMR F. Mellinger, M. Wilhelm, P. Belik, H. Schwind, H.W. Spiess; Macromol. Chem. Phys. 200 2454 (1999)
Rheologische Charakterisierung von Materialien im nichtlinearen Bereich bei Anwendung oszillatorischer Verscherungen M. Wilhelm, P. Reinheimer, M. Ortseifer, H.W. Spiess; Kautsch. Gummi Kunstst. 52 754 (1999)
Combined reduced 4D 13C exchange and 1H spin diffusion experiment for determing the length scale of dynamic heterogeneities U. Tracht, M. Wilhelm, A. Heuer, H.W. Spiess; J. Magn. Reson. 140 460 (1999)
Calibration of 1H-NMR spin diffusion coefficents for mobile polymers through transverse relaxation measurements F. Mellinger, M. Wilhelm, H.W. Spiess; Macromolecules 32 4686 (1999)
High sensitivity Fourier-Transform Rheology M. Wilhelm, P. Reinheimer, M. Ortseifer; Rheol. Acta 38 349-356 (1999)
A collection of solid-state 13C CP/MAS NMR spectra of common polymers M. Wilhelm, M. Neidhöfer, S. Spiegel, H.W. Spiess; Macromol. Chem. Phys. 200 2205 (1999)
Quantitative Measurement of Core Coverage in Core-Shell Particles by Solid State 1H-NMR Spin-Diffusion Experiments F. Mellinger, M. Wilhelm, H.W. Spiess, R. Baumstark, A. Haunschild; Macromol. Chem. Phys. 200 719 (1999)
Articles 1998
Energy landscapes of interacting randomly and periodically charged rigid polyampholytes S. Panyukov, Y. Rabin, M. Wilhelm; Acta Polymer. 49 544 (1998)
Length scales of the glass transition as determined by multidimensional NMR U. Tracht, M. Wilhelm, A. Heuer, H. Feng, K. Schmidt-Rohr, H.W. Spiess; Phys. Rev. Letters 81 2727 (1998)
2D CP/MAS 13C Isotropic Chemical Shift Correlation established by 1H Spin Diffusion M. Wilhelm, H. Feng, U. Tracht, H.W. Spiess; J. Magn. Reson. 134 255 (1998)
Nature of the non-exponential primary relaxation in structural glass-formers probed by dynamically selective experiments R. Böhmer, R.V. Chambelin, G. Diezemann, B. Geil, A. Heuer, G. Hinze, S.C. Kuebler, R. Richert, B. Schiener, H. Sillescu, H.W. Spiess, U. Tracht, M. Wilhelm; J. Non-Cryst. Solids (Vigo Proceedings) 235 1 (1998)
Fourier-Transform Rheology M. Wilhelm, P. Reinheimer, D. Maring, H.W. Spiess; Progress and Trends in Rheology; Portoroz Proceedings; Steinkopf-Springer 127 (1998)
Fourier-Transform Rheology M. Wilhelm, D. Maring, H.W. Spiess; Rheol. Acta 37 399-405 (1998)
Solid State NMR Studies of Structure and Dynamics of Erucamide/isotactic-Poly(propylene) Blends I. Quijada-Garrido, M. Wilhelm, H.W. Spiess, J.M. Barrales-Rienda; Macromol. Chem. Phys. 199 985 (1998)
Structure of water-containing latexes: Remagnetization effects during solid-state NMR spin-diffusion experiments F. Mellinger, M. Wilhelm, K. Landfester, H.W. Spiess, A. Haunschild, J. Packusch; Acta Polymer. 49 108 (1998)
Articles 1997 and earlier
Site-Hopping Dynamics of Benzene Adsorbed on Ca-LSX Zeolite Studied by Solid-State Exchange 13C NMR D.J. Schaefer, D.E. Favre, M. Wilhelm, S.J. Weigel, B.F. Chmelka; J. Am. Chem. Soc. 119 9252 (1997)
Detection of slow 180° Phenylene Flips in PET-Fibres via 13C Two-dimensional Solid-State Exchange NMR M. Wilhelm, H.W. Spiess;
Macromolecules 29 1088 (1996)
Rate Memory of Structural Relaxations in Glasses and its Detection by Multidimensional NMR A. Heuer, M. Wilhelm, H. Zimmermann, H.W. Spiess; Phys. Rev. Letters 75 2851 (1995)
Dynamics of Benzene Absorbed on Ca-LSX Zeolite Studied by Solid-State Two-Dimensional Exchange 13C NMR M. Wilhelm, A. Firouzi, D.E. Favre, L.M. Bull, D. Schaefer, B.F. Chmelka; J. Am. Chem. Soc. 117 2923 (1995)
Detection of dynamics and phase separation in polymers using 2D 1H NMR in solids M. Wilhelm, S. Lehmann, C. Jäger, H.W. Spiess, R. Jerome; Magn. Reson. Chem. 32 3 (1994)
New 2D 13C Methods (DECODER) for Evaluation of Orientation Distribution in Polymer Fibres and Films M. Wilhelm, K. Schmidt-Rohr, H.W. Spiess, B.F. Chmelka; GIT Fachz. Lab.; 38 946 (1994)
The orientation distribution in an industrial sample of poly(p-phenyleneterephthalamide) determined by two- and three dimensional NMR techniques M. Wilhelm, S. Féaux de Lacroix, J.J. Titman, K. Schmidt-Rohr, H.W. Spiess; Acta Polymer. 44 279 (1993)
Determination of Chemical-Shift Tensors Orientation in Methylene Groups by Separated-Local-Field NMR K. Schmidt-Rohr, M. Wilhelm, A. Johannson, H.W. Spiess; Magn. Reson. Chem. 31 352 (1993)
Poly(styrene-ethylene oxide) Block Copolymer Micelle Formation in Water: A fluorescence Probe Study M. Wilhelm, C. Zhao, Y. Wang, R. Xu, M.A. Winnik, J. Mura, G. Riess, M. Croucher; Macromolecules 24 1033 (1991)